Sonochemical synthesis and characterization of lead sulfide nanoparticles

Sonochemical synthesis and characterization of lead sulfide nanoparticles

Large-scale PbS nanoparticles were successfully synthesized by a sonochemical method using Pb(CH3COO)2·H2O and CH3CSNH2 as lead and sulfur sources in ethylene glycol as solvent. The structure, morphology and phase of the PbS nanoparticles were characterized by X-ray diffraction (XRD), transmission e...

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Main Authors: Anukorn Phuruangrata, Somchai Thongtem, Titipun Thongtem, Budsabong Kuntalue
Format: Journal
Published: 2018
Subjects:
Biochemistry, Genetics and Molecular Biology
Chemistry
Engineering
Materials Science
Physics and Astronomy
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866534275&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/51356
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-513562018-09-04T06:14:00Z Sonochemical synthesis and characterization of lead sulfide nanoparticles Anukorn Phuruangrata Somchai Thongtem Titipun Thongtem Budsabong Kuntalue Biochemistry, Genetics and Molecular Biology Chemistry Engineering Materials Science Physics and Astronomy Large-scale PbS nanoparticles were successfully synthesized by a sonochemical method using Pb(CH3COO)2·H2O and CH3CSNH2 as lead and sulfur sources in ethylene glycol as solvent. The structure, morphology and phase of the PbS nanoparticles were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), energy dispersive X-ray (EDX) spectroscopy and photoluminescence (PL) spectroscopy. They were found that the as-synthesized products were cubic structured PbS nanoparticles. By using 254 nm excitation wavelength, the nanoparticles show an emission peak at 390 nm. The formation mechanism of these PbS nanocrystals was also proposed in this report. 2018-09-04T06:00:44Z 2018-09-04T06:00:44Z 2012-09-27 Journal 18423582 2-s2.0-84866534275 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866534275&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51356
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Biochemistry, Genetics and Molecular Biology
Chemistry
Engineering
Materials Science
Physics and Astronomy
spellingShingle Biochemistry, Genetics and Molecular Biology
Chemistry
Engineering
Materials Science
Physics and Astronomy
Anukorn Phuruangrata
Somchai Thongtem
Titipun Thongtem
Budsabong Kuntalue
Sonochemical synthesis and characterization of lead sulfide nanoparticles
description Large-scale PbS nanoparticles were successfully synthesized by a sonochemical method using Pb(CH3COO)2·H2O and CH3CSNH2 as lead and sulfur sources in ethylene glycol as solvent. The structure, morphology and phase of the PbS nanoparticles were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), energy dispersive X-ray (EDX) spectroscopy and photoluminescence (PL) spectroscopy. They were found that the as-synthesized products were cubic structured PbS nanoparticles. By using 254 nm excitation wavelength, the nanoparticles show an emission peak at 390 nm. The formation mechanism of these PbS nanocrystals was also proposed in this report.
format Journal
author Anukorn Phuruangrata
Somchai Thongtem
Titipun Thongtem
Budsabong Kuntalue
author_facet Anukorn Phuruangrata
Somchai Thongtem
Titipun Thongtem
Budsabong Kuntalue
author_sort Anukorn Phuruangrata
title Sonochemical synthesis and characterization of lead sulfide nanoparticles
title_short Sonochemical synthesis and characterization of lead sulfide nanoparticles
title_full Sonochemical synthesis and characterization of lead sulfide nanoparticles
title_fullStr Sonochemical synthesis and characterization of lead sulfide nanoparticles
title_full_unstemmed Sonochemical synthesis and characterization of lead sulfide nanoparticles
title_sort sonochemical synthesis and characterization of lead sulfide nanoparticles
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866534275&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/51356
_version_ 1681423755002249216

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