Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands
The microwave-assisted SNAr reaction of 2,4,6-trichloro-1,3,5- triazine with various unprotected amino acids was developed for the synthesis of C3-symmetrical polycarboxylate ligands which can be used as structural directing units in metal-organic frameworks. The reactions were performed in water us...
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th-cmuir.6653943832-513712018-09-04T06:13:16Z Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands Weeranuch Karuehanon Watcharee Fanfuenha Apinpus Rujiwatra Mookda Pattarawarapan Biochemistry, Genetics and Molecular Biology Chemistry Pharmacology, Toxicology and Pharmaceutics The microwave-assisted SNAr reaction of 2,4,6-trichloro-1,3,5- triazine with various unprotected amino acids was developed for the synthesis of C3-symmetrical polycarboxylate ligands which can be used as structural directing units in metal-organic frameworks. The reactions were performed in water using a domestic microwave oven as the heating device. In comparison to the reactions performed under conventional heating, the reactions under microwave irradiation proceeded much more rapidly within 20 min to afford the desired ligands in comparative yields to those obtained by conventional heating. © 2012 Elsevier Ltd. All rights reserved. 2018-09-04T06:00:58Z 2018-09-04T06:00:58Z 2012-07-04 Journal 18733581 00404039 2-s2.0-84861646559 10.1016/j.tetlet.2012.04.124 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84861646559&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51371 |
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Biochemistry, Genetics and Molecular Biology Chemistry Pharmacology, Toxicology and Pharmaceutics Weeranuch Karuehanon Watcharee Fanfuenha Apinpus Rujiwatra Mookda Pattarawarapan Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands |
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The microwave-assisted SNAr reaction of 2,4,6-trichloro-1,3,5- triazine with various unprotected amino acids was developed for the synthesis of C3-symmetrical polycarboxylate ligands which can be used as structural directing units in metal-organic frameworks. The reactions were performed in water using a domestic microwave oven as the heating device. In comparison to the reactions performed under conventional heating, the reactions under microwave irradiation proceeded much more rapidly within 20 min to afford the desired ligands in comparative yields to those obtained by conventional heating. © 2012 Elsevier Ltd. All rights reserved. |
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Journal |
author |
Weeranuch Karuehanon Watcharee Fanfuenha Apinpus Rujiwatra Mookda Pattarawarapan |
author_facet |
Weeranuch Karuehanon Watcharee Fanfuenha Apinpus Rujiwatra Mookda Pattarawarapan |
author_sort |
Weeranuch Karuehanon |
title |
Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands |
title_short |
Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands |
title_full |
Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands |
title_fullStr |
Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands |
title_full_unstemmed |
Microwave-assisted S NAr reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of C 3-symmetrical polycarboxylate ligands |
title_sort |
microwave-assisted s nar reaction of 2,4,6-trichloro-1,3,5- triazine for the rapid synthesis of c 3-symmetrical polycarboxylate ligands |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84861646559&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51371 |
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