Synthesis of CuS with different morphologies by refluxing method: Nanopaticles in clusters and nanoflakes in spongelike clusters
Clusters of CuS nanoparticles and sponge-like structures of CuS nanoflakes were synthesized by refluxing method at a temperature of 130 °C for 1.5-6 h using copper chloride (CuCl 2·4H 2O) and thioacetamide (CH 3CSNH...
Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Journal |
| Published: |
2018
|
| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84868324001&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51472 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Institution: | Chiang Mai University |
| Summary: | Clusters of CuS nanoparticles and sponge-like structures of CuS nanoflakes were synthesized by refluxing method at a temperature of 130 °C for 1.5-6 h using copper chloride (CuCl 2·4H 2O) and thioacetamide (CH 3CSNH 2) as starting materials in deionized water to form [Cu(CH 3CSNH 2) 2]Cl 2 complexes, specified by thermogravimetric, CHNS/O and Fourier transform inferred analyses. Phase and morphology were investigated by powder X-ray diffraction and scanning electron microscopy. |
|---|