Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent

Antimony sulfide (Sb 2S 3) was successfully synthesized from antimony chloride (SbCl 3) and sodium thiosulfate (Na 2S 2O 3) in ethylene glycol (EG) containi...

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Main Authors:	Jutarat Kavinchan, Titipun Thongtem, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Chemistry Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866393300&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51478
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-51478
record_format	dspace
spelling	th-cmuir.6653943832-514782018-09-04T06:14:03Z Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent Jutarat Kavinchan Titipun Thongtem Somchai Thongtem Chemistry Materials Science Physics and Astronomy Antimony sulfide (Sb 2S 3) was successfully synthesized from antimony chloride (SbCl 3) and sodium thiosulfate (Na 2S 2O 3) in ethylene glycol (EG) containing different contents of cetyltrimethylammonium bromide (CTAB) as a template and splitting agent by the 600 W cyclic microwave radiation (CMR). X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopy and photoluminescence (PL) spectroscopy revealed the presence of only orthorhombic Sb 2S 3 phase in the shape of twin flowers of single crystalline square nanorod petals, growing along the [001] direction, including the vibration peaks that were in accordance with those of the stibnite with the 435 nm violet wavelength emission peaks. 2018-09-04T06:02:42Z 2018-09-04T06:02:42Z 2012-09-01 Journal 15848663 2-s2.0-84866393300 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866393300&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51478
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Chemistry Materials Science Physics and Astronomy
spellingShingle	Chemistry Materials Science Physics and Astronomy Jutarat Kavinchan Titipun Thongtem Somchai Thongtem Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
description	Antimony sulfide (Sb 2S 3) was successfully synthesized from antimony chloride (SbCl 3) and sodium thiosulfate (Na 2S 2O 3) in ethylene glycol (EG) containing different contents of cetyltrimethylammonium bromide (CTAB) as a template and splitting agent by the 600 W cyclic microwave radiation (CMR). X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopy and photoluminescence (PL) spectroscopy revealed the presence of only orthorhombic Sb 2S 3 phase in the shape of twin flowers of single crystalline square nanorod petals, growing along the [001] direction, including the vibration peaks that were in accordance with those of the stibnite with the 435 nm violet wavelength emission peaks.
format	Journal
author	Jutarat Kavinchan Titipun Thongtem Somchai Thongtem
author_facet	Jutarat Kavinchan Titipun Thongtem Somchai Thongtem
author_sort	Jutarat Kavinchan
title	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_short	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_full	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_fullStr	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_full_unstemmed	Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent
title_sort	cyclic microwave assisted synthesis of sb 2s 3 twin flowers in solutions containing a template and splitting agent
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84866393300&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51478
_version_	1681423776960479232

Cyclic microwave assisted synthesis of Sb 2S 3 twin flowers in solutions containing a template and splitting agent

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