A two-stage solid-state reaction to lead zirconate titanate powders
An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite ph...
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2014
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th-cmuir.6653943832-51592014-08-30T02:56:13Z A two-stage solid-state reaction to lead zirconate titanate powders Chaisan W. Khamman O. Yimnirun R. Ananta S. An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3 and PbTiO3 phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase. 2014-08-30T02:56:13Z 2014-08-30T02:56:13Z 2007 Conference Paper 00150193 10.1080/00150190701512763 79199 FEROA http://www.scopus.com/inward/record.url?eid=2-s2.0-75449085131&partnerID=40&md5=01586ddf68e4d8f8c55a670bc37be73c http://cmuir.cmu.ac.th/handle/6653943832/5159 English |
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Thailand |
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English |
| description |
An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3 and PbTiO3 phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase. |
| format |
Conference or Workshop Item |
| author |
Chaisan W. Khamman O. Yimnirun R. Ananta S. |
| spellingShingle |
Chaisan W. Khamman O. Yimnirun R. Ananta S. A two-stage solid-state reaction to lead zirconate titanate powders |
| author_facet |
Chaisan W. Khamman O. Yimnirun R. Ananta S. |
| author_sort |
Chaisan W. |
| title |
A two-stage solid-state reaction to lead zirconate titanate powders |
| title_short |
A two-stage solid-state reaction to lead zirconate titanate powders |
| title_full |
A two-stage solid-state reaction to lead zirconate titanate powders |
| title_fullStr |
A two-stage solid-state reaction to lead zirconate titanate powders |
| title_full_unstemmed |
A two-stage solid-state reaction to lead zirconate titanate powders |
| title_sort |
two-stage solid-state reaction to lead zirconate titanate powders |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-75449085131&partnerID=40&md5=01586ddf68e4d8f8c55a670bc37be73c http://cmuir.cmu.ac.th/handle/6653943832/5159 |
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1681420372645249024 |