Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method

Cubic and star-shaped dendritic PbS structures were successfully synthesized by the 120 °C and 10 h solvothermal reactions of lead nitrate and sulfur sources (thiourea and thiosemicarbazide). XRD, SEM and TEM analyses revealed the presence of pure cubic PbS phase with different morphologies, control...

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Main Authors:	Anukorn Phuruangrat, Titipun Thongtem, Budsabong Kuntalue, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Engineering Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84862158360&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51605
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Institution:	Chiang Mai University

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spelling	th-cmuir.6653943832-516052018-09-04T06:14:05Z Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method Anukorn Phuruangrat Titipun Thongtem Budsabong Kuntalue Somchai Thongtem Engineering Materials Science Physics and Astronomy Cubic and star-shaped dendritic PbS structures were successfully synthesized by the 120 °C and 10 h solvothermal reactions of lead nitrate and sulfur sources (thiourea and thiosemicarbazide). XRD, SEM and TEM analyses revealed the presence of pure cubic PbS phase with different morphologies, controlled by the sulfur sources. Cubic and star-shaped dendritic PbS crystals were respectively synthesized in the solutions containing thiourea and thiosemicarbazide as sulfur sources. Possible formation mechanisms of cubic and star-shaped dendritic PbS structures were also proposed. © 2012 Elsevier B.V. All rights reserved. 2018-09-04T06:05:16Z 2018-09-04T06:05:16Z 2012-08-15 Journal 0167577X 2-s2.0-84862158360 10.1016/j.matlet.2012.04.129 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84862158360&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51605
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Engineering Materials Science Physics and Astronomy
spellingShingle	Engineering Materials Science Physics and Astronomy Anukorn Phuruangrat Titipun Thongtem Budsabong Kuntalue Somchai Thongtem Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method
description	Cubic and star-shaped dendritic PbS structures were successfully synthesized by the 120 °C and 10 h solvothermal reactions of lead nitrate and sulfur sources (thiourea and thiosemicarbazide). XRD, SEM and TEM analyses revealed the presence of pure cubic PbS phase with different morphologies, controlled by the sulfur sources. Cubic and star-shaped dendritic PbS crystals were respectively synthesized in the solutions containing thiourea and thiosemicarbazide as sulfur sources. Possible formation mechanisms of cubic and star-shaped dendritic PbS structures were also proposed. © 2012 Elsevier B.V. All rights reserved.
format	Journal
author	Anukorn Phuruangrat Titipun Thongtem Budsabong Kuntalue Somchai Thongtem
author_facet	Anukorn Phuruangrat Titipun Thongtem Budsabong Kuntalue Somchai Thongtem
author_sort	Anukorn Phuruangrat
title	Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method
title_short	Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method
title_full	Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method
title_fullStr	Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method
title_full_unstemmed	Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method
title_sort	characterization of cubic and star-shaped dendritic pbs structures synthesized by a solvothermal method
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84862158360&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51605
_version_	1681423799879204864

Characterization of cubic and star-shaped dendritic PbS structures synthesized by a solvothermal method

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