Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method

Hierarchical tree-like wurtzite CdS nanostructure was successfully synthesized by the 200°C and 24 h solvothermal reaction of cadmium nitrate and thiourea as starting materials in 1:1 volume ratio of diethylenetriamine and ethylenediamine as a mixed solvent. Phase and morphology of the as-synthesize...

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Main Authors: Anukorn Phuruangrat, Titipun Thongtem, Somchai Thongtem
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/51608
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-516082018-09-04T06:14:05Z Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Engineering Materials Science Physics and Astronomy Hierarchical tree-like wurtzite CdS nanostructure was successfully synthesized by the 200°C and 24 h solvothermal reaction of cadmium nitrate and thiourea as starting materials in 1:1 volume ratio of diethylenetriamine and ethylenediamine as a mixed solvent. Phase and morphology of the as-synthesized CdS product were characterized by X-ray diffraction (XRD), Raman spectroscopy and transmission electron microscopy (TEM), including its photonic absorption by UV-visible spectroscopy. XRD spectrum and TEM image showed hexagonal wurtzite CdS structure with a 1-2 μm prototypical cluster, composed of a number of limbed nanorods. Its Raman spectrum was specified as the first-order (1LO) and second-order (2LO) longitudinal optical phonon modes at 298 and 599 cm- 1. UV-visible spectrum shows an absorption peak centered at around 489 nm, assigned as the excitonic transition, blue shifted comparing to its bulk. © 2012 Elsevier B.V. All rights reserved. 2018-09-04T06:05:18Z 2018-09-04T06:05:18Z 2012-08-01 Journal 0167577X 2-s2.0-84861581819 10.1016/j.matlet.2012.04.089 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84861581819&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51608
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
Physics and Astronomy
spellingShingle Engineering
Materials Science
Physics and Astronomy
Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method
description Hierarchical tree-like wurtzite CdS nanostructure was successfully synthesized by the 200°C and 24 h solvothermal reaction of cadmium nitrate and thiourea as starting materials in 1:1 volume ratio of diethylenetriamine and ethylenediamine as a mixed solvent. Phase and morphology of the as-synthesized CdS product were characterized by X-ray diffraction (XRD), Raman spectroscopy and transmission electron microscopy (TEM), including its photonic absorption by UV-visible spectroscopy. XRD spectrum and TEM image showed hexagonal wurtzite CdS structure with a 1-2 μm prototypical cluster, composed of a number of limbed nanorods. Its Raman spectrum was specified as the first-order (1LO) and second-order (2LO) longitudinal optical phonon modes at 298 and 599 cm- 1. UV-visible spectrum shows an absorption peak centered at around 489 nm, assigned as the excitonic transition, blue shifted comparing to its bulk. © 2012 Elsevier B.V. All rights reserved.
format Journal
author Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
author_facet Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
author_sort Anukorn Phuruangrat
title Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method
title_short Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method
title_full Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method
title_fullStr Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method
title_full_unstemmed Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method
title_sort characterization and photonic absorption of hierarchical tree-like cds nanostructure synthesized by solvothermal method
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84861581819&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/51608
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