Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method
Hierarchical tree-like wurtzite CdS nanostructure was successfully synthesized by the 200°C and 24 h solvothermal reaction of cadmium nitrate and thiourea as starting materials in 1:1 volume ratio of diethylenetriamine and ethylenediamine as a mixed solvent. Phase and morphology of the as-synthesize...
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th-cmuir.6653943832-516082018-09-04T06:14:05Z Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Engineering Materials Science Physics and Astronomy Hierarchical tree-like wurtzite CdS nanostructure was successfully synthesized by the 200°C and 24 h solvothermal reaction of cadmium nitrate and thiourea as starting materials in 1:1 volume ratio of diethylenetriamine and ethylenediamine as a mixed solvent. Phase and morphology of the as-synthesized CdS product were characterized by X-ray diffraction (XRD), Raman spectroscopy and transmission electron microscopy (TEM), including its photonic absorption by UV-visible spectroscopy. XRD spectrum and TEM image showed hexagonal wurtzite CdS structure with a 1-2 μm prototypical cluster, composed of a number of limbed nanorods. Its Raman spectrum was specified as the first-order (1LO) and second-order (2LO) longitudinal optical phonon modes at 298 and 599 cm- 1. UV-visible spectrum shows an absorption peak centered at around 489 nm, assigned as the excitonic transition, blue shifted comparing to its bulk. © 2012 Elsevier B.V. All rights reserved. 2018-09-04T06:05:18Z 2018-09-04T06:05:18Z 2012-08-01 Journal 0167577X 2-s2.0-84861581819 10.1016/j.matlet.2012.04.089 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84861581819&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51608 |
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Engineering Materials Science Physics and Astronomy Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method |
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Hierarchical tree-like wurtzite CdS nanostructure was successfully synthesized by the 200°C and 24 h solvothermal reaction of cadmium nitrate and thiourea as starting materials in 1:1 volume ratio of diethylenetriamine and ethylenediamine as a mixed solvent. Phase and morphology of the as-synthesized CdS product were characterized by X-ray diffraction (XRD), Raman spectroscopy and transmission electron microscopy (TEM), including its photonic absorption by UV-visible spectroscopy. XRD spectrum and TEM image showed hexagonal wurtzite CdS structure with a 1-2 μm prototypical cluster, composed of a number of limbed nanorods. Its Raman spectrum was specified as the first-order (1LO) and second-order (2LO) longitudinal optical phonon modes at 298 and 599 cm- 1. UV-visible spectrum shows an absorption peak centered at around 489 nm, assigned as the excitonic transition, blue shifted comparing to its bulk. © 2012 Elsevier B.V. All rights reserved. |
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author |
Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
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Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
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Anukorn Phuruangrat |
title |
Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method |
title_short |
Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method |
title_full |
Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method |
title_fullStr |
Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method |
title_full_unstemmed |
Characterization and photonic absorption of hierarchical tree-like CdS nanostructure synthesized by solvothermal method |
title_sort |
characterization and photonic absorption of hierarchical tree-like cds nanostructure synthesized by solvothermal method |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84861581819&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51608 |
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