Characterization of nano-rod ZnWO4 prepared by surfactant-assisting solvothermal reaction
Nano-rod ZnWO4 was solvothermally prepared by the reaction of Zn(CH3COO)22H2O with Na2(WO 4).2H2O in water at 150-200°C using the pH of 5.0, 7.0, 9.0 and 12.0 for 24, 48 and 72 h. N-cetyl pyridinium chloride was used as a surfactant. By using XRD, SAED, EDX and TEM, nano-rod ZnWO4 containing Zn, W a...
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Conference or Workshop Item |
| Language: | English |
| Published: |
2014
|
| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-38349166469&partnerID=40&md5=17ec1005ab74c340936b07f97c896b77 http://cmuir.cmu.ac.th/handle/6653943832/5166 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Institution: | Chiang Mai University |
| Language: | English |
| Summary: | Nano-rod ZnWO4 was solvothermally prepared by the reaction of Zn(CH3COO)22H2O with Na2(WO 4).2H2O in water at 150-200°C using the pH of 5.0, 7.0, 9.0 and 12.0 for 24, 48 and 72 h. N-cetyl pyridinium chloride was used as a surfactant. By using XRD, SAED, EDX and TEM, nano-rod ZnWO4 containing Zn, W and O was detected. The pH values can play a role in the length of the nano-rods and their crystallinities. FTIR revealed the presence of Zn-O-W, W-O and Zn-O stretching vibrations of the products. Their photoluminescent (PL) spectra are similar and the wavelengths at the highest intensities were detected over the range of 445-450 nm. |
|---|