Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites

Nanocrystalline Cu0.5Co0.5Fe2O4powders were prepared via a metal-cellulose precursor synthetic route. Cellulose was used as a fuel and a dispersing agent. The resulting precursors were calcined in the temperature range of 450-600 °C. The phase development of the samples was determined by using Fouri...

Full description

Saved in:
Bibliographic Details
Main Authors: Kontad Ounnunkad, Sukon Phanichphant
Format: Journal
Published: 2018
Subjects:
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84855685012&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/51664
Tags: Add Tag
No Tags, Be the first to tag this record!
Institution: Chiang Mai University
id th-cmuir.6653943832-51664
record_format dspace
spelling th-cmuir.6653943832-516642018-09-04T06:14:33Z Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites Kontad Ounnunkad Sukon Phanichphant Engineering Materials Science Physics and Astronomy Nanocrystalline Cu0.5Co0.5Fe2O4powders were prepared via a metal-cellulose precursor synthetic route. Cellulose was used as a fuel and a dispersing agent. The resulting precursors were calcined in the temperature range of 450-600 °C. The phase development of the samples was determined by using Fourier transform infrared (FT-IR) spectroscopy and powder X-ray diffraction (XRD). The field-dependent magnetizations of the nanopowders were measured by vibrating sample magnetometer (VSM). All XRD patterns are of a spinel ferrite with cubic symmetry. Microstructure of the ferrites showed irregular shapes and uniform particles with agglomeration. From XRD data, the crystallite sizes are in range of 16-42 nm. Saturation magnetization and coercivity increased with increasing calcining temperature due to enhancement of crystallinity and reduction of oxygen vacancies. © 2011 Elsevier Ltd. All rights reserved. 2018-09-04T06:05:52Z 2018-09-04T06:05:52Z 2012-02-01 Journal 00255408 2-s2.0-84855685012 10.1016/j.materresbull.2011.10.012 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84855685012&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/51664
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
Physics and Astronomy
spellingShingle Engineering
Materials Science
Physics and Astronomy
Kontad Ounnunkad
Sukon Phanichphant
Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites
description Nanocrystalline Cu0.5Co0.5Fe2O4powders were prepared via a metal-cellulose precursor synthetic route. Cellulose was used as a fuel and a dispersing agent. The resulting precursors were calcined in the temperature range of 450-600 °C. The phase development of the samples was determined by using Fourier transform infrared (FT-IR) spectroscopy and powder X-ray diffraction (XRD). The field-dependent magnetizations of the nanopowders were measured by vibrating sample magnetometer (VSM). All XRD patterns are of a spinel ferrite with cubic symmetry. Microstructure of the ferrites showed irregular shapes and uniform particles with agglomeration. From XRD data, the crystallite sizes are in range of 16-42 nm. Saturation magnetization and coercivity increased with increasing calcining temperature due to enhancement of crystallinity and reduction of oxygen vacancies. © 2011 Elsevier Ltd. All rights reserved.
format Journal
author Kontad Ounnunkad
Sukon Phanichphant
author_facet Kontad Ounnunkad
Sukon Phanichphant
author_sort Kontad Ounnunkad
title Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites
title_short Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites
title_full Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites
title_fullStr Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites
title_full_unstemmed Cellulose-precursor synthesis of nanocrystalline Co 0.5Cu 0.5Fe 2O 4 spinel ferrites
title_sort cellulose-precursor synthesis of nanocrystalline co 0.5cu 0.5fe 2o 4 spinel ferrites
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84855685012&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/51664
_version_ 1681423810521202688