Characterization of orthorhombic α-MoO<inf>3</inf>microplates produced by a microwave plasma process

Orthorhombic α-MoO3microplates were produced from (NH4)6Mo7O24̇4H2O solid powder by a 900 W microwave plasma for 40, 50, and 60min. Phase, morphologies, and vibration modes were characterized by X-ray diffraction (XRD), selected area electron diffraction (SAED), scanning electron microscopy (SEM), a...

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Bibliographic Details
Main Authors: Arrak Klinbumrung, Titipun Thongtem, Somchai Thongtem
Format: Journal
Published: 2018
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Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84858187885&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/51761
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Institution: Chiang Mai University
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Summary:Orthorhombic α-MoO3microplates were produced from (NH4)6Mo7O24̇4H2O solid powder by a 900 W microwave plasma for 40, 50, and 60min. Phase, morphologies, and vibration modes were characterized by X-ray diffraction (XRD), selected area electron diffraction (SAED), scanning electron microscopy (SEM), and Raman and Fourier transform infrared (FTIR) spectroscopy. Sixty min processing resulted in the best crystallization of the α-MoO3phase, with photoluminescence (PL) in a wavelength range of 430-440nm. © 2012 Arrak Klinbumrung et al.