Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process
Mixtures of (CH3COO)2Mg·4H2O and (NH4)6Mo7O24·4H2O containing 0.7, 1.0 and 1.3 g of poly(vinyl alcohol) (PVA, 125,000 MW) were electrospun by +15 kV direct voltage to form fibrous webs. In the present research, the fibrous web of the 1.3 g PVA was characterized by a thermogravimetric analyser (TGA),...
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th-cmuir.6653943832-523932018-09-04T09:36:51Z Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process Surangkana Wannapop Titipun Thongtem Somchai Thongtem Chemistry Materials Science Physics and Astronomy Mixtures of (CH3COO)2Mg·4H2O and (NH4)6Mo7O24·4H2O containing 0.7, 1.0 and 1.3 g of poly(vinyl alcohol) (PVA, 125,000 MW) were electrospun by +15 kV direct voltage to form fibrous webs. In the present research, the fibrous web of the 1.3 g PVA was characterized by a thermogravimetric analyser (TGA), and calcined at 400-600 °C for 3 h. MgMoO4contained in the fibrous webs was characterized by X-ray diffraction (XRD), morphologies of the webs by scanning and transmission electron microscopy (SEM, TEM) and atomic force microscopy (AFM), and their vibration modes by Fourier transform infrared (FTIR) and Raman spectrometry. The 5.15 eV direct energy gap, caused by the electronic transition in the (MoO4)2-complex, was determined by UV-visible absorption. Formation mechanism of the fibrous webs was also proposed according to the experimental results. © 2013 Elsevier Ltd. 2018-09-04T09:24:35Z 2018-09-04T09:24:35Z 2013-05-01 Journal 00223697 2-s2.0-84874658407 10.1016/j.jpcs.2013.01.002 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84874658407&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/52393 |
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Chemistry Materials Science Physics and Astronomy Surangkana Wannapop Titipun Thongtem Somchai Thongtem Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process |
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Mixtures of (CH3COO)2Mg·4H2O and (NH4)6Mo7O24·4H2O containing 0.7, 1.0 and 1.3 g of poly(vinyl alcohol) (PVA, 125,000 MW) were electrospun by +15 kV direct voltage to form fibrous webs. In the present research, the fibrous web of the 1.3 g PVA was characterized by a thermogravimetric analyser (TGA), and calcined at 400-600 °C for 3 h. MgMoO4contained in the fibrous webs was characterized by X-ray diffraction (XRD), morphologies of the webs by scanning and transmission electron microscopy (SEM, TEM) and atomic force microscopy (AFM), and their vibration modes by Fourier transform infrared (FTIR) and Raman spectrometry. The 5.15 eV direct energy gap, caused by the electronic transition in the (MoO4)2-complex, was determined by UV-visible absorption. Formation mechanism of the fibrous webs was also proposed according to the experimental results. © 2013 Elsevier Ltd. |
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author |
Surangkana Wannapop Titipun Thongtem Somchai Thongtem |
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Surangkana Wannapop Titipun Thongtem Somchai Thongtem |
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Surangkana Wannapop |
title |
Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process |
title_short |
Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process |
title_full |
Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process |
title_fullStr |
Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process |
title_full_unstemmed |
Fabrication of MgMoO4-PVA and MgMoO4 fibrous webs via a direct high voltage electrospinning process |
title_sort |
fabrication of mgmoo4-pva and mgmoo4 fibrous webs via a direct high voltage electrospinning process |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84874658407&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/52393 |
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