One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites
Zn4Sb3nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-r...
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| Main Authors: | , , , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84887095364&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/52519 |
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| Institution: | Chiang Mai University |
| Summary: | Zn4Sb3nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-ray (EDX) spectroscopy, transmission electron microscopy (TEM), Raman spectroscopy and UV-visible spectroscopy. In this research, Zn4Sb3nanocrystals with a prominent vibration mode at 144 cm-1and 1.22 eV optical band gap were detected, including Zn4Sb3-ZnSb composites were also synthesized using microwave plasma for 10 min. © 2013 Elsevier Ltd. All rights reserved. |
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