One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites
Zn4Sb3nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-r...
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th-cmuir.6653943832-525192018-09-04T09:36:17Z One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites Sudarat Sitthichai Titipun Thongtem Somchai Thongtem Tawat Suriwong Engineering Materials Science Physics and Astronomy Zn4Sb3nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-ray (EDX) spectroscopy, transmission electron microscopy (TEM), Raman spectroscopy and UV-visible spectroscopy. In this research, Zn4Sb3nanocrystals with a prominent vibration mode at 144 cm-1and 1.22 eV optical band gap were detected, including Zn4Sb3-ZnSb composites were also synthesized using microwave plasma for 10 min. © 2013 Elsevier Ltd. All rights reserved. 2018-09-04T09:26:34Z 2018-09-04T09:26:34Z 2013-11-11 Journal 10963677 07496036 2-s2.0-84887095364 10.1016/j.spmi.2013.10.004 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84887095364&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/52519 |
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Engineering Materials Science Physics and Astronomy |
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Engineering Materials Science Physics and Astronomy Sudarat Sitthichai Titipun Thongtem Somchai Thongtem Tawat Suriwong One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites |
| description |
Zn4Sb3nanocrystals were synthesized by a 900 W microwave of 4.5:3 M ratio Zn:Sb with a total mass of 1 g for 5 min. Phase, internal texture, constituents, vibration mode and energy gap were detected using X-ray diffraction (XRD), scanning electron microscopy (SEM) equipped with energy dispersive X-ray (EDX) spectroscopy, transmission electron microscopy (TEM), Raman spectroscopy and UV-visible spectroscopy. In this research, Zn4Sb3nanocrystals with a prominent vibration mode at 144 cm-1and 1.22 eV optical band gap were detected, including Zn4Sb3-ZnSb composites were also synthesized using microwave plasma for 10 min. © 2013 Elsevier Ltd. All rights reserved. |
| format |
Journal |
| author |
Sudarat Sitthichai Titipun Thongtem Somchai Thongtem Tawat Suriwong |
| author_facet |
Sudarat Sitthichai Titipun Thongtem Somchai Thongtem Tawat Suriwong |
| author_sort |
Sudarat Sitthichai |
| title |
One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites |
| title_short |
One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites |
| title_full |
One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites |
| title_fullStr |
One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites |
| title_full_unstemmed |
One-step synthesis of Zn<inf>4</inf>Sb<inf>3</inf>nanocrystals and Zn<inf>4</inf>Sb<inf>3</inf>-ZnSb composites |
| title_sort |
one-step synthesis of zn<inf>4</inf>sb<inf>3</inf>nanocrystals and zn<inf>4</inf>sb<inf>3</inf>-znsb composites |
| publishDate |
2018 |
| url |
https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84887095364&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/52519 |
| _version_ |
1681423965799579648 |