Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders

xPb(Zr1/2Ti1/2)O3-(1-x)Pb(Zn1/3Nb2/3)O3or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn2Nb34O87precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, particle size and che...

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Main Authors: Penphitcha Amonpattaratkit, Supon Ananta
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/52688
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-526882018-09-04T09:37:05Z Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders Penphitcha Amonpattaratkit Supon Ananta Materials Science Physics and Astronomy xPb(Zr1/2Ti1/2)O3-(1-x)Pb(Zn1/3Nb2/3)O3or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn2Nb34O87precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, particle size and chemical composition of perovskite ferroelectric powders in the solid solution of PZT-PZN system were investigated. Perovskite phase transition from a tetragonal to a coexistence of tetragonal and rhombohedral phases occurred as composition and firing temperature change. The tetragonality factor and degree of spherical grain shape were observed to increase with increasing PZT content. Moreover, the degree of agglomeration and averaged particle size of the PZT-PZN powders were also found to increase at higher calcination temperatures. © 2013 Copyright Taylor and Francis Group, LLC. 2018-09-04T09:30:35Z 2018-09-04T09:30:35Z 2013-01-01 Journal 15635112 00150193 2-s2.0-84891821328 10.1080/00150193.2013.846128 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891821328&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/52688
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Materials Science
Physics and Astronomy
spellingShingle Materials Science
Physics and Astronomy
Penphitcha Amonpattaratkit
Supon Ananta
Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
description xPb(Zr1/2Ti1/2)O3-(1-x)Pb(Zn1/3Nb2/3)O3or xPZT-(1-x)PZN (x = 0.85-0.95)powders were prepared by a modified mixed-oxide synthetic route via a combination of Zn2Nb34O87precursor and rapid vibro-milling techniques. Effects of calcination temperature on phase formation, morphology, particle size and chemical composition of perovskite ferroelectric powders in the solid solution of PZT-PZN system were investigated. Perovskite phase transition from a tetragonal to a coexistence of tetragonal and rhombohedral phases occurred as composition and firing temperature change. The tetragonality factor and degree of spherical grain shape were observed to increase with increasing PZT content. Moreover, the degree of agglomeration and averaged particle size of the PZT-PZN powders were also found to increase at higher calcination temperatures. © 2013 Copyright Taylor and Francis Group, LLC.
format Journal
author Penphitcha Amonpattaratkit
Supon Ananta
author_facet Penphitcha Amonpattaratkit
Supon Ananta
author_sort Penphitcha Amonpattaratkit
title Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_short Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_full Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_fullStr Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_full_unstemmed Synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
title_sort synthesis, formation and characterization of lead zirconate titanate-lead zinc niobate powders
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891821328&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/52688
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