Effects of process parameter and excess Bi<inf>2</inf>O<inf>3</inf>on phase formation and electrical properties of BiFeO<inf>3</inf>ceramics
The BiFeO3was prepared by a mixed oxide, solid-state reaction method. Excess Bi2O3(1-7wt%) was introduced prior to powder calcination to compensate for any Bi2O3that may have been lost from the samples due to volatilization during heat treatments. Various heating rates (1-10°C/min) were performed at...
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| Main Authors: | , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84891750584&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/52704 |
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| Institution: | Chiang Mai University |
| Summary: | The BiFeO3was prepared by a mixed oxide, solid-state reaction method. Excess Bi2O3(1-7wt%) was introduced prior to powder calcination to compensate for any Bi2O3that may have been lost from the samples due to volatilization during heat treatments. Various heating rates (1-10°C/min) were performed at the calcination state. X-ray diffraction analysis revealed that pure phase BFO was observed for the samples calcined at a low heating rate (1°C/min) and contained lower amount of Bi2O3.The higher levels of excess Bi2O3produced an increased in dielectric constant and dielectric loss. Further, ferroelectric behavior was improved for higher amount Bi2O3contented samples. © 2013 Copyright Taylor and Francis Group, LLC. |
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