Sonocatalyzed ammonothermal preparation of fine lithium niobate powders
The so-called sonocatalyzed ammonothermal technique has been developed for the preparation of lithium niobate fine powders from commercially as-received niobium pentoxide and lithium nitrate. The present work shows that the application of ultrasonic activation prior to the ammonothermal treatment ca...
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2014
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th-cmuir.6653943832-53792014-08-30T02:56:28Z Sonocatalyzed ammonothermal preparation of fine lithium niobate powders Rujiwatra A. Thammajak N. Chimupala Y. Laoratanakul P. The so-called sonocatalyzed ammonothermal technique has been developed for the preparation of lithium niobate fine powders from commercially as-received niobium pentoxide and lithium nitrate. The present work shows that the application of ultrasonic activation prior to the ammonothermal treatment can produce a single phase lithium niobate fine powder at a relatively low temperature of 220°C. The influences of Li-precursors, ammonia solution concentration, reaction temperature and time, as well as Li:Nb mole ratio - which is evidentially the most critical factor promoting a single phase formation - are discussed. © 2008 Trans Tech Publications, Switzerland. 2014-08-30T02:56:28Z 2014-08-30T02:56:28Z 2008 Conference Paper 9780878493562 10226680 75596 http://www.scopus.com/inward/record.url?eid=2-s2.0-62949242484&partnerID=40&md5=74df71a752f3aa3abbf78e170da0e39e http://cmuir.cmu.ac.th/handle/6653943832/5379 English |
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The so-called sonocatalyzed ammonothermal technique has been developed for the preparation of lithium niobate fine powders from commercially as-received niobium pentoxide and lithium nitrate. The present work shows that the application of ultrasonic activation prior to the ammonothermal treatment can produce a single phase lithium niobate fine powder at a relatively low temperature of 220°C. The influences of Li-precursors, ammonia solution concentration, reaction temperature and time, as well as Li:Nb mole ratio - which is evidentially the most critical factor promoting a single phase formation - are discussed. © 2008 Trans Tech Publications, Switzerland. |
format |
Conference or Workshop Item |
author |
Rujiwatra A. Thammajak N. Chimupala Y. Laoratanakul P. |
spellingShingle |
Rujiwatra A. Thammajak N. Chimupala Y. Laoratanakul P. Sonocatalyzed ammonothermal preparation of fine lithium niobate powders |
author_facet |
Rujiwatra A. Thammajak N. Chimupala Y. Laoratanakul P. |
author_sort |
Rujiwatra A. |
title |
Sonocatalyzed ammonothermal preparation of fine lithium niobate powders |
title_short |
Sonocatalyzed ammonothermal preparation of fine lithium niobate powders |
title_full |
Sonocatalyzed ammonothermal preparation of fine lithium niobate powders |
title_fullStr |
Sonocatalyzed ammonothermal preparation of fine lithium niobate powders |
title_full_unstemmed |
Sonocatalyzed ammonothermal preparation of fine lithium niobate powders |
title_sort |
sonocatalyzed ammonothermal preparation of fine lithium niobate powders |
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2014 |
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http://www.scopus.com/inward/record.url?eid=2-s2.0-62949242484&partnerID=40&md5=74df71a752f3aa3abbf78e170da0e39e http://cmuir.cmu.ac.th/handle/6653943832/5379 |
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