Microwave-assisted synthesis, characterization and photoluminescence of shuttle-like BaMoO<inf>4</inf>microstructure
© 2015 Wroclaw University of Technology. Shuttle-like BaMoO4microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent containing 20 mL 5 M NaOH by microwave radiation at 180 W for 30 min. The as-synthesized BaMoO4product was...
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| Main Authors: | , , , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84945924382&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/54481 |
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| Institution: | Chiang Mai University |
| Summary: | © 2015 Wroclaw University of Technology. Shuttle-like BaMoO4microstructure has been successfully synthesized from Ba(N03)2·4H20 and Na2MoO4·2H2O as starting materials in ethylene glycol solvent containing 20 mL 5 M NaOH by microwave radiation at 180 W for 30 min. The as-synthesized BaMoO4product was characterized by X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy, Raman spectrophotometry, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and photolumines-cence (PL) spectroscopy. XRD patterns revealed that the products was tetragonal BaMoO4phase. SEM and TEM characterization showed that the product had a shuttle-like BaMoO4microstructure. PL of the shuttle-like BaMoO4microstructure showed a maximum emission at 466 nm excited by 280 nm wavelength. |
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