Preparation of flower-like PbS nano-structures using cyclic microwave radiation
Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The...
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
2014
|
| Online Access: | http://www.scopus.com/inward/record.url?eid=2-s2.0-53249107976&partnerID=40&md5=a09cb577e15d79cb10bbf02019fe64d8 http://cmuir.cmu.ac.th/handle/6653943832/5465 |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| Institution: | Chiang Mai University |
| Language: | English |
| id |
th-cmuir.6653943832-5465 |
|---|---|
| record_format |
dspace |
| spelling |
th-cmuir.6653943832-54652014-08-30T02:56:33Z Preparation of flower-like PbS nano-structures using cyclic microwave radiation Thongtem T. Phuruangrat A. Thongtem S. Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The experimental and simulated patterns are in good accord. A Raman spectrometer revealed the presence of vibrations at 134, 275 and 431 cm-1. Flower-like PbS nano-structures were also characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM), although the products were prepared using different mole ratios of the starting agents. 2014-08-30T02:56:33Z 2014-08-30T02:56:33Z 2008 Article 12299162 http://www.scopus.com/inward/record.url?eid=2-s2.0-53249107976&partnerID=40&md5=a09cb577e15d79cb10bbf02019fe64d8 http://cmuir.cmu.ac.th/handle/6653943832/5465 English |
| institution |
Chiang Mai University |
| building |
Chiang Mai University Library |
| country |
Thailand |
| collection |
CMU Intellectual Repository |
| language |
English |
| description |
Flower-like PbS nano-structures were successfully prepared from different mole ratios of Pb(NO3)2 to CH5N3S in propylene glycol, using the cyclic process of 600 W microwave power for 15 minutes. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The experimental and simulated patterns are in good accord. A Raman spectrometer revealed the presence of vibrations at 134, 275 and 431 cm-1. Flower-like PbS nano-structures were also characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM), although the products were prepared using different mole ratios of the starting agents. |
| format |
Article |
| author |
Thongtem T. Phuruangrat A. Thongtem S. |
| spellingShingle |
Thongtem T. Phuruangrat A. Thongtem S. Preparation of flower-like PbS nano-structures using cyclic microwave radiation |
| author_facet |
Thongtem T. Phuruangrat A. Thongtem S. |
| author_sort |
Thongtem T. |
| title |
Preparation of flower-like PbS nano-structures using cyclic microwave radiation |
| title_short |
Preparation of flower-like PbS nano-structures using cyclic microwave radiation |
| title_full |
Preparation of flower-like PbS nano-structures using cyclic microwave radiation |
| title_fullStr |
Preparation of flower-like PbS nano-structures using cyclic microwave radiation |
| title_full_unstemmed |
Preparation of flower-like PbS nano-structures using cyclic microwave radiation |
| title_sort |
preparation of flower-like pbs nano-structures using cyclic microwave radiation |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-53249107976&partnerID=40&md5=a09cb577e15d79cb10bbf02019fe64d8 http://cmuir.cmu.ac.th/handle/6653943832/5465 |
| _version_ |
1681420430874771456 |