Characterization of PbS with different morphologies produced using a cyclic microwave radiation

PbS was produced from different lead (Pb(CH3COO)2·H2O, PbCl2·2.5H2O, Pb(NO3)2) and sulfur (CH3CSNH2, CH5N3S, NH2CSNH2) sources in propylene glycol using a cyclic microwave radiation at different powers and prolonged times. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area elec...

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Main Authors: Phuruangrat A., Thongtem T., Thongtem S.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-51449109844&partnerID=40&md5=b46c639ab31953a61c495de2d712ec28
http://cmuir.cmu.ac.th/handle/6653943832/5482
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spelling th-cmuir.6653943832-54822014-08-30T02:56:35Z Characterization of PbS with different morphologies produced using a cyclic microwave radiation Phuruangrat A. Thongtem T. Thongtem S. PbS was produced from different lead (Pb(CH3COO)2·H2O, PbCl2·2.5H2O, Pb(NO3)2) and sulfur (CH3CSNH2, CH5N3S, NH2CSNH2) sources in propylene glycol using a cyclic microwave radiation at different powers and prolonged times. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED) techniques. The interpreted and simulated patterns are in good accord. Raman spectrometer revealed the presence of vibrations at 138, 273 and 439 cm-1. Different morphologies (nano-sized particles, hexapods, cubes, ferns and magic squares) were characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM). The product morphologies were influenced by the starting agents, microwave powers and prolonged times. © 2008 Elsevier B.V. All rights reserved. 2014-08-30T02:56:35Z 2014-08-30T02:56:35Z 2008 Article 01694332 10.1016/j.apsusc.2008.01.059 ASUSE http://www.scopus.com/inward/record.url?eid=2-s2.0-51449109844&partnerID=40&md5=b46c639ab31953a61c495de2d712ec28 http://cmuir.cmu.ac.th/handle/6653943832/5482 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description PbS was produced from different lead (Pb(CH3COO)2·H2O, PbCl2·2.5H2O, Pb(NO3)2) and sulfur (CH3CSNH2, CH5N3S, NH2CSNH2) sources in propylene glycol using a cyclic microwave radiation at different powers and prolonged times. PbS (cubic) was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED) techniques. The interpreted and simulated patterns are in good accord. Raman spectrometer revealed the presence of vibrations at 138, 273 and 439 cm-1. Different morphologies (nano-sized particles, hexapods, cubes, ferns and magic squares) were characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM). The product morphologies were influenced by the starting agents, microwave powers and prolonged times. © 2008 Elsevier B.V. All rights reserved.
format Article
author Phuruangrat A.
Thongtem T.
Thongtem S.
spellingShingle Phuruangrat A.
Thongtem T.
Thongtem S.
Characterization of PbS with different morphologies produced using a cyclic microwave radiation
author_facet Phuruangrat A.
Thongtem T.
Thongtem S.
author_sort Phuruangrat A.
title Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_short Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_full Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_fullStr Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_full_unstemmed Characterization of PbS with different morphologies produced using a cyclic microwave radiation
title_sort characterization of pbs with different morphologies produced using a cyclic microwave radiation
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-51449109844&partnerID=40&md5=b46c639ab31953a61c495de2d712ec28
http://cmuir.cmu.ac.th/handle/6653943832/5482
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