Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process
Li1-x Ni1+x O2 was prepared by the thermal-assisted precipitation process of LiOH • H2O and Ni(CH3COO)2 • 4H2O at a pH of 6-13 followed by the high temperature calcination for a variety of prolonged times. Phases, morphologies and constituents were characterized using an x-ray diffractometer (XRD),...
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th-cmuir.6653943832-55922014-08-30T02:56:42Z Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process Thongtem T. Sitthikhankaew R. Thongtem S. Li1-x Ni1+x O2 was prepared by the thermal-assisted precipitation process of LiOH • H2O and Ni(CH3COO)2 • 4H2O at a pH of 6-13 followed by the high temperature calcination for a variety of prolonged times. Phases, morphologies and constituents were characterized using an x-ray diffractometer (XRD), a scanning electron microscope (SEM), an energy dispersive x-ray (EDX) analyzer an atomic absorption spectrophotometer (AAS) and titration. Maximum [I(003)/I(104)] and minimum [I (006+102)/I(101)] intensity ratios were used to determine the preparation conditions. In addition, possible formation reactions of the precursors and calcined products were proposed. © 2008 MAIK Nauka. 2014-08-30T02:56:42Z 2014-08-30T02:56:42Z 2008 Article 00360236 10.1134/S0036023608040050 RJICA http://www.scopus.com/inward/record.url?eid=2-s2.0-43149085262&partnerID=40&md5=9fa3812dec361dedd0bb72b2ffca0577 http://cmuir.cmu.ac.th/handle/6653943832/5592 English |
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Li1-x Ni1+x O2 was prepared by the thermal-assisted precipitation process of LiOH • H2O and Ni(CH3COO)2 • 4H2O at a pH of 6-13 followed by the high temperature calcination for a variety of prolonged times. Phases, morphologies and constituents were characterized using an x-ray diffractometer (XRD), a scanning electron microscope (SEM), an energy dispersive x-ray (EDX) analyzer an atomic absorption spectrophotometer (AAS) and titration. Maximum [I(003)/I(104)] and minimum [I (006+102)/I(101)] intensity ratios were used to determine the preparation conditions. In addition, possible formation reactions of the precursors and calcined products were proposed. © 2008 MAIK Nauka. |
| format |
Article |
| author |
Thongtem T. Sitthikhankaew R. Thongtem S. |
| spellingShingle |
Thongtem T. Sitthikhankaew R. Thongtem S. Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process |
| author_facet |
Thongtem T. Sitthikhankaew R. Thongtem S. |
| author_sort |
Thongtem T. |
| title |
Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process |
| title_short |
Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process |
| title_full |
Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process |
| title_fullStr |
Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process |
| title_full_unstemmed |
Characterization of Li1-x Ni1+x O2 prepared by the thermal-assisted precipitation process |
| title_sort |
characterization of li1-x ni1+x o2 prepared by the thermal-assisted precipitation process |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-43149085262&partnerID=40&md5=9fa3812dec361dedd0bb72b2ffca0577 http://cmuir.cmu.ac.th/handle/6653943832/5592 |
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1681420454648086528 |