Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process

Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process

© 2016, Springer Science+Business Media Dordrecht. Solutions containing zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and potassium titanium oxalate dihydrate (C4K2O9Ti·2H2O) with different molar ratios of Zn:Ti at a pH of 10 were hydrothermally processed at 120, 160, and 200 °C to form ZnO–anatase, ZnO–...

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Main Authors: Jirapong Arin, Somchai Thongtem, Anukorn Phuruangrat, Titipun Thongtem
Format: Journal
Published: 2018
Subjects:
Chemistry
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/56984
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-569842018-09-05T03:33:09Z Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process Jirapong Arin Somchai Thongtem Anukorn Phuruangrat Titipun Thongtem Chemistry © 2016, Springer Science+Business Media Dordrecht. Solutions containing zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and potassium titanium oxalate dihydrate (C4K2O9Ti·2H2O) with different molar ratios of Zn:Ti at a pH of 10 were hydrothermally processed at 120, 160, and 200 °C to form ZnO–anatase, ZnO–anatase–rutile and ZnO–rutile nanocomposites. Upon subsequent calcination the precursors at high temperatures, ZnTiO3, Zn2TiO4, and Zn2Ti3O8nanoparticles were synthesized. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectroscopy, Raman spectrophotometry, and photoluminescence (PL) spectroscopy revealed the existence of nanocomposites and nanoparticles with strong emission at 386 nm for Zn2TiO4and Zn2Ti3O8and at 370 nm for ZnTiO3. 2018-09-05T03:33:09Z 2018-09-05T03:33:09Z 2017-05-01 Journal 15685675 09226168 2-s2.0-84997272259 10.1007/s11164-016-2818-y https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84997272259&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/56984
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Chemistry
spellingShingle Chemistry
Jirapong Arin
Somchai Thongtem
Anukorn Phuruangrat
Titipun Thongtem
Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process
description © 2016, Springer Science+Business Media Dordrecht. Solutions containing zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and potassium titanium oxalate dihydrate (C4K2O9Ti·2H2O) with different molar ratios of Zn:Ti at a pH of 10 were hydrothermally processed at 120, 160, and 200 °C to form ZnO–anatase, ZnO–anatase–rutile and ZnO–rutile nanocomposites. Upon subsequent calcination the precursors at high temperatures, ZnTiO3, Zn2TiO4, and Zn2Ti3O8nanoparticles were synthesized. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), selected area electron diffraction (SAED), Fourier transform infrared (FTIR) spectroscopy, Raman spectrophotometry, and photoluminescence (PL) spectroscopy revealed the existence of nanocomposites and nanoparticles with strong emission at 386 nm for Zn2TiO4and Zn2Ti3O8and at 370 nm for ZnTiO3.
format Journal
author Jirapong Arin
Somchai Thongtem
Anukorn Phuruangrat
Titipun Thongtem
author_facet Jirapong Arin
Somchai Thongtem
Anukorn Phuruangrat
Titipun Thongtem
author_sort Jirapong Arin
title Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process
title_short Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process
title_full Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process
title_fullStr Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process
title_full_unstemmed Characterization of ZnO–TiO<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process
title_sort characterization of zno–tio<inf>2</inf>and zinc titanate nanoparticles synthesized by hydrothermal process
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84997272259&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/56984
_version_ 1681424794162036736

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