Phase formation investigation in PZT materials by Synchrotron X-ray absorption spectroscopy techniques

Phase formation investigation in PZT materials by Synchrotron X-ray absorption spectroscopy techniques

© 2017 Taylor & Francis Group, LLC. PbZr1-xTixO3(PZT) powders (x = 0.45–0.54) were synthesized by conventional solid state reaction method. The phase information was investigated by a combination of X-ray diffraction and X-ray absorption spectroscopy (XAS) techniques. The XRD measurements indi...

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Bibliographic Details
Main Authors: Kanjana Suponok, Jaru Jutimoosik, Atipong Bootchanont, Pinit Kidkhunthod, Athipong Ngamjarurojana, Saroj Rujirawat, Rattikorn Yimnirun
Format: Journal
Published: 2018
Subjects:
Engineering
Materials Science
Physics and Astronomy
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=85015970071&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/57349
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Institution: Chiang Mai University
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Summary:© 2017 Taylor & Francis Group, LLC. PbZr1-xTixO3(PZT) powders (x = 0.45–0.54) were synthesized by conventional solid state reaction method. The phase information was investigated by a combination of X-ray diffraction and X-ray absorption spectroscopy (XAS) techniques. The XRD measurements indicated the global phase formation of the prepared powders was the mixture of rhombohedral and tetragonal phases. However, the local phase formation around titanium atom was revealed using X-ray Absorption Near-Edge Structure (XANES), indicating the existence of monoclinic phase within the compositional range studied.

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