Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide

Nanostructured AgBiS2 with the shapes of flowers and hexapods was successfully produced from AgNO3, BiCl3 and sulfur sources (thioacetamide and thiourea) in ethylene glycol, by a cyclic microwave process. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SA...

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Main Authors: Thongtem T., Jaroenchaichana J., Thongtem S.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-68349131613&partnerID=40&md5=9b203e7fec6248055487e22efee59a06
http://cmuir.cmu.ac.th/handle/6653943832/5792
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Institution: Chiang Mai University
Language: English
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spelling th-cmuir.6653943832-57922014-08-30T03:23:28Z Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide Thongtem T. Jaroenchaichana J. Thongtem S. Nanostructured AgBiS2 with the shapes of flowers and hexapods was successfully produced from AgNO3, BiCl3 and sulfur sources (thioacetamide and thiourea) in ethylene glycol, by a cyclic microwave process. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Their SAED patterns were also in accordance with those of the simulations. Scanning and transmission electron microscopies (SEM and TEM) revealed the gradual transformation of nanostructured flowers into nanostructured hexapods, due to the microwave power increases. Their photoluminescence (PL) emissions were detected at the same wavelength of 435 nm, although they were produced under different conditions. © 2009 Elsevier B.V. All rights reserved. 2014-08-30T03:23:28Z 2014-08-30T03:23:28Z 2009 Article 0167577X 10.1016/j.matlet.2009.07.009 MLETD http://www.scopus.com/inward/record.url?eid=2-s2.0-68349131613&partnerID=40&md5=9b203e7fec6248055487e22efee59a06 http://cmuir.cmu.ac.th/handle/6653943832/5792 English
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description Nanostructured AgBiS2 with the shapes of flowers and hexapods was successfully produced from AgNO3, BiCl3 and sulfur sources (thioacetamide and thiourea) in ethylene glycol, by a cyclic microwave process. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Their SAED patterns were also in accordance with those of the simulations. Scanning and transmission electron microscopies (SEM and TEM) revealed the gradual transformation of nanostructured flowers into nanostructured hexapods, due to the microwave power increases. Their photoluminescence (PL) emissions were detected at the same wavelength of 435 nm, although they were produced under different conditions. © 2009 Elsevier B.V. All rights reserved.
format Article
author Thongtem T.
Jaroenchaichana J.
Thongtem S.
spellingShingle Thongtem T.
Jaroenchaichana J.
Thongtem S.
Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
author_facet Thongtem T.
Jaroenchaichana J.
Thongtem S.
author_sort Thongtem T.
title Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_short Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_full Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_fullStr Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_full_unstemmed Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_sort cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
publishDate 2014
url http://www.scopus.com/inward/record.url?eid=2-s2.0-68349131613&partnerID=40&md5=9b203e7fec6248055487e22efee59a06
http://cmuir.cmu.ac.th/handle/6653943832/5792
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