Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation
BaMoO4 and BaWO4 nanocrystals were synthesized from Ba(NO3)2 and Na2MeO4 (Me=Mo and W) solutions using 50% of 600 W microwave irradiation for 20 min. The products were characterized using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electr...
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th-cmuir.6653943832-58752014-08-30T03:23:34Z Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation Phuruangrat A. Thongtem T. Thongtem S. BaMoO4 and BaWO4 nanocrystals were synthesized from Ba(NO3)2 and Na2MeO4 (Me=Mo and W) solutions using 50% of 600 W microwave irradiation for 20 min. The products were characterized using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and photoluminescence (PL) spectrophotometry. They show that the products are good dispersed nanocrystals (poly-nanocrystals) of single-phase scheelite tetragonal structure with the vibration modes corresponding to the molybdate and tungstate compounds. Their photoluminescence was detected at 415 and 392 nm for BaMoO4 and BaWO4, respectively. © 2009 Elsevier Ltd. All rights reserved. 2014-08-30T03:23:34Z 2014-08-30T03:23:34Z 2009 Article 00223697 10.1016/j.jpcs.2009.05.006 JPCSA http://www.scopus.com/inward/record.url?eid=2-s2.0-67649311419&partnerID=40&md5=04fb42c6b91b22448f7d03859533fd9f http://cmuir.cmu.ac.th/handle/6653943832/5875 English |
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BaMoO4 and BaWO4 nanocrystals were synthesized from Ba(NO3)2 and Na2MeO4 (Me=Mo and W) solutions using 50% of 600 W microwave irradiation for 20 min. The products were characterized using X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), selected area electron diffraction (SAED) and photoluminescence (PL) spectrophotometry. They show that the products are good dispersed nanocrystals (poly-nanocrystals) of single-phase scheelite tetragonal structure with the vibration modes corresponding to the molybdate and tungstate compounds. Their photoluminescence was detected at 415 and 392 nm for BaMoO4 and BaWO4, respectively. © 2009 Elsevier Ltd. All rights reserved. |
| format |
Article |
| author |
Phuruangrat A. Thongtem T. Thongtem S. |
| spellingShingle |
Phuruangrat A. Thongtem T. Thongtem S. Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation |
| author_facet |
Phuruangrat A. Thongtem T. Thongtem S. |
| author_sort |
Phuruangrat A. |
| title |
Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation |
| title_short |
Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation |
| title_full |
Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation |
| title_fullStr |
Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation |
| title_full_unstemmed |
Barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation |
| title_sort |
barium molybdate and barium tungstate nanocrystals synthesized by a cyclic microwave irradiation |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-67649311419&partnerID=40&md5=04fb42c6b91b22448f7d03859533fd9f http://cmuir.cmu.ac.th/handle/6653943832/5875 |
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