Effect of vibro-milling time on phase formation and particle size of barium titanate nanopowders

Barium titanate (BT) nanopowder was synthesized by a solid state reaction via a rapid vibro-milling technique. The effect of milling time on phase formation and particle size of BT powder was investigated. Powder samples were characterized using XRD (X-ray diffraction) and SEM techniques. It was fou...

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Bibliographic Details
Main Authors: W. Chaisan, R. Yimnirun, S. Ananta
Format: Journal
Published: 2018
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Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=55949132905&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/59444
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Institution: Chiang Mai University
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Summary:Barium titanate (BT) nanopowder was synthesized by a solid state reaction via a rapid vibro-milling technique. The effect of milling time on phase formation and particle size of BT powder was investigated. Powder samples were characterized using XRD (X-ray diffraction) and SEM techniques. It was found that the resulting BT powders have a range of particle size depending on milling times. Production of a single-phase BT nanopowder can be successfully achieved by employing a combination of 30 h milling time and calcination conditions of 1200 °C for 2 h. © 2008 Elsevier Ltd and Techna Group S.r.l.