Synthesis of lead molybdate and lead tungstate via microwave irradiation method

Nanocrystallines lead molybdate and lead tungstate were successfully prepared by microwave irradiation method. The products were characterized by XRD, Raman spectroscopy, TEM and luminescence spectroscopy. The phase of products were detected by XRD and was in accordance with that of the XRD simulati...

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Main Authors:	Anukorn Phuruangrat, Titipun Thongtem, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Chemistry Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=68049126285&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/59466
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Institution:	Chiang Mai University

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spelling	th-cmuir.6653943832-594662018-09-10T03:24:49Z Synthesis of lead molybdate and lead tungstate via microwave irradiation method Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Chemistry Materials Science Physics and Astronomy Nanocrystallines lead molybdate and lead tungstate were successfully prepared by microwave irradiation method. The products were characterized by XRD, Raman spectroscopy, TEM and luminescence spectroscopy. The phase of products were detected by XRD and was in accordance with that of the XRD simulation using CaRIne Version 3.1 program. TEM showed the particle sizes of 15-50 nm for PbMoO4and 12-32 nm for PbWO4. Their photoluminescent spectra were decomposed to four individual Gaussian components in blue and green wavelength range for PbMoO4and three individual Gaussian components in blue wavelength range for PbWO4. These photoluminescent features could be interpreted by Jahn-Teller splitting effect on [MO4]2-(M{double bond, long}Ma and W) tetrahedrons. © 2009 Elsevier B.V. All rights reserved. 2018-09-10T03:15:40Z 2018-09-10T03:15:40Z 2009-08-01 Journal 00220248 2-s2.0-68049126285 10.1016/j.jcrysgro.2009.06.013 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=68049126285&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/59466
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Chemistry Materials Science Physics and Astronomy
spellingShingle	Chemistry Materials Science Physics and Astronomy Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Synthesis of lead molybdate and lead tungstate via microwave irradiation method
description	Nanocrystallines lead molybdate and lead tungstate were successfully prepared by microwave irradiation method. The products were characterized by XRD, Raman spectroscopy, TEM and luminescence spectroscopy. The phase of products were detected by XRD and was in accordance with that of the XRD simulation using CaRIne Version 3.1 program. TEM showed the particle sizes of 15-50 nm for PbMoO4and 12-32 nm for PbWO4. Their photoluminescent spectra were decomposed to four individual Gaussian components in blue and green wavelength range for PbMoO4and three individual Gaussian components in blue wavelength range for PbWO4. These photoluminescent features could be interpreted by Jahn-Teller splitting effect on [MO4]2-(M{double bond, long}Ma and W) tetrahedrons. © 2009 Elsevier B.V. All rights reserved.
format	Journal
author	Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem
author_facet	Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem
author_sort	Anukorn Phuruangrat
title	Synthesis of lead molybdate and lead tungstate via microwave irradiation method
title_short	Synthesis of lead molybdate and lead tungstate via microwave irradiation method
title_full	Synthesis of lead molybdate and lead tungstate via microwave irradiation method
title_fullStr	Synthesis of lead molybdate and lead tungstate via microwave irradiation method
title_full_unstemmed	Synthesis of lead molybdate and lead tungstate via microwave irradiation method
title_sort	synthesis of lead molybdate and lead tungstate via microwave irradiation method
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=68049126285&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/59466
_version_	1681425256530575360

Synthesis of lead molybdate and lead tungstate via microwave irradiation method

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