Effect of vibro-milling time on phase formation and particle size of barium titanate nanopowders

Barium titanate (BT) nanopowder was synthesized by a solid state reaction via a rapid vibro-milling technique. The effect of milling time on phase formation and particle size of BT powder was investigated. Powder samples were characterized using XRD (X-ray diffraction) and SEM techniques. It was fou...

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Bibliographic Details
Main Authors: Chaisan W., Yimnirun R., Ananta S.
Format: Article
Language:English
Published: 2014
Online Access:http://www.scopus.com/inward/record.url?eid=2-s2.0-55949132905&partnerID=40&md5=d218f5a6bd68876dd43a3e3b1e1c2fcd
http://cmuir.cmu.ac.th/handle/6653943832/5952
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Institution: Chiang Mai University
Language: English
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Summary:Barium titanate (BT) nanopowder was synthesized by a solid state reaction via a rapid vibro-milling technique. The effect of milling time on phase formation and particle size of BT powder was investigated. Powder samples were characterized using XRD (X-ray diffraction) and SEM techniques. It was found that the resulting BT powders have a range of particle size depending on milling times. Production of a single-phase BT nanopowder can be successfully achieved by employing a combination of 30 h milling time and calcination conditions of 1200 °C for 2 h. © 2008 Elsevier Ltd and Techna Group S.r.l.