Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide

Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide

Nanostructured AgBiS2with the shapes of flowers and hexapods was successfully produced from AgNO3, BiCl3and sulfur sources (thioacetamide and thiourea) in ethylene glycol, by a cyclic microwave process. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED...

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Main Authors: Titipun Thongtem, Jadesada Jaroenchaichana, Somchai Thongtem
Format: Journal
Published: 2018
Subjects:
Engineering
Materials Science
Physics and Astronomy
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=68349131613&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/59569
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-595692018-09-10T03:24:36Z Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide Titipun Thongtem Jadesada Jaroenchaichana Somchai Thongtem Engineering Materials Science Physics and Astronomy Nanostructured AgBiS2with the shapes of flowers and hexapods was successfully produced from AgNO3, BiCl3and sulfur sources (thioacetamide and thiourea) in ethylene glycol, by a cyclic microwave process. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Their SAED patterns were also in accordance with those of the simulations. Scanning and transmission electron microscopies (SEM and TEM) revealed the gradual transformation of nanostructured flowers into nanostructured hexapods, due to the microwave power increases. Their photoluminescence (PL) emissions were detected at the same wavelength of 435 nm, although they were produced under different conditions. © 2009 Elsevier B.V. All rights reserved. 2018-09-10T03:17:23Z 2018-09-10T03:17:23Z 2009-10-15 Journal 0167577X 2-s2.0-68349131613 10.1016/j.matlet.2009.07.009 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=68349131613&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/59569
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
Physics and Astronomy
spellingShingle Engineering
Materials Science
Physics and Astronomy
Titipun Thongtem
Jadesada Jaroenchaichana
Somchai Thongtem
Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
description Nanostructured AgBiS2with the shapes of flowers and hexapods was successfully produced from AgNO3, BiCl3and sulfur sources (thioacetamide and thiourea) in ethylene glycol, by a cyclic microwave process. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Their SAED patterns were also in accordance with those of the simulations. Scanning and transmission electron microscopies (SEM and TEM) revealed the gradual transformation of nanostructured flowers into nanostructured hexapods, due to the microwave power increases. Their photoluminescence (PL) emissions were detected at the same wavelength of 435 nm, although they were produced under different conditions. © 2009 Elsevier B.V. All rights reserved.
format Journal
author Titipun Thongtem
Jadesada Jaroenchaichana
Somchai Thongtem
author_facet Titipun Thongtem
Jadesada Jaroenchaichana
Somchai Thongtem
author_sort Titipun Thongtem
title Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_short Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_full Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_fullStr Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_full_unstemmed Cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
title_sort cyclic microwave-assisted synthesis of flower-like and hexapod silver bismuth sulfide
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=68349131613&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/59569
_version_ 1681425275631435776

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