Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis

Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis

Different morphologies of PbS were prepared using microwave-assisted synthesis of 1:4, 1:1 and 4:1 molar ratios of Pb(CH3COO)2to NH2CSNH2in propylene glycol. Cubic PbS was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Raman spectrometry revealed the presence o...

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Main Authors: Anukorn Phuruangrat, Titipun Thongtem, Somchai Thongtem
Format: Journal
Published: 2018
Subjects:
Engineering
Materials Science
Physics and Astronomy
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=58649096122&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/59594
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-595942018-09-10T03:25:17Z Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Engineering Materials Science Physics and Astronomy Different morphologies of PbS were prepared using microwave-assisted synthesis of 1:4, 1:1 and 4:1 molar ratios of Pb(CH3COO)2to NH2CSNH2in propylene glycol. Cubic PbS was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Raman spectrometry revealed the presence of vibrations at 134, 274 and 430 cm- 1. The product morphologies for different molar ratios of Pb(CH3COO)2to NH2CSNH2were also characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM). The obtained morphologies changed with molar ratios used for the starting agents. The simulated diffraction pattern was also in accordance with the interpretation of the experimental results. © 2008 Elsevier B.V. All rights reserved. 2018-09-10T03:17:46Z 2018-09-10T03:17:46Z 2009-03-31 Journal 0167577X 2-s2.0-58649096122 10.1016/j.matlet.2008.12.029 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=58649096122&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/59594
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Engineering
Materials Science
Physics and Astronomy
spellingShingle Engineering
Materials Science
Physics and Astronomy
Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis
description Different morphologies of PbS were prepared using microwave-assisted synthesis of 1:4, 1:1 and 4:1 molar ratios of Pb(CH3COO)2to NH2CSNH2in propylene glycol. Cubic PbS was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). Raman spectrometry revealed the presence of vibrations at 134, 274 and 430 cm- 1. The product morphologies for different molar ratios of Pb(CH3COO)2to NH2CSNH2were also characterized using a scanning electron microscope (SEM) and a transmission electron microscope (TEM). The obtained morphologies changed with molar ratios used for the starting agents. The simulated diffraction pattern was also in accordance with the interpretation of the experimental results. © 2008 Elsevier B.V. All rights reserved.
format Journal
author Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
author_facet Anukorn Phuruangrat
Titipun Thongtem
Somchai Thongtem
author_sort Anukorn Phuruangrat
title Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis
title_short Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis
title_full Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis
title_fullStr Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis
title_full_unstemmed Preparation of ear-like, hexapod and dendritic PbS using cyclic microwave-assisted synthesis
title_sort preparation of ear-like, hexapod and dendritic pbs using cyclic microwave-assisted synthesis
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=58649096122&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/59594
_version_ 1681425280248315904

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