Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents
CdS (hcp) was solvothermally synthesized from different Cd and S sources (Cd(NO3)2, CdCl2, Cd(CH3COO)2, (NH4)2S, CH3CSNH2, NH2CSNH2and CH5N3S) at 200 °C in mixed solvents of ethylenediamine and butylamine. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (S...
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th-cmuir.6653943832-597032018-09-10T03:25:09Z Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Materials Science Physics and Astronomy CdS (hcp) was solvothermally synthesized from different Cd and S sources (Cd(NO3)2, CdCl2, Cd(CH3COO)2, (NH4)2S, CH3CSNH2, NH2CSNH2and CH5N3S) at 200 °C in mixed solvents of ethylenediamine and butylamine. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The SAED pattern is in accordance with that of the simulation. Scanning and transmission electron microscopies (SEM and TEM) revealed the presence of different products consisting of nano-wires, nano-rods and tetra-pods controlled by Cd and S sources. High resolution TEM (HRTEM) showed that the products grew in [0 0 1] direction that was both parallel with and normal to their (1 0 0) and (0 0 2) planes, respectively. Raman spectra showed the same fundamental and overtone modes at 300 and 600 cm-1, respectively. © 2009 Elsevier B.V. All rights reserved. 2018-09-10T03:19:56Z 2018-09-10T03:19:56Z 2009-05-01 Journal 15671739 2-s2.0-67349172558 10.1016/j.cap.2009.01.041 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=67349172558&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/59703 |
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Materials Science Physics and Astronomy Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents |
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CdS (hcp) was solvothermally synthesized from different Cd and S sources (Cd(NO3)2, CdCl2, Cd(CH3COO)2, (NH4)2S, CH3CSNH2, NH2CSNH2and CH5N3S) at 200 °C in mixed solvents of ethylenediamine and butylamine. The phase was detected using X-ray diffraction (XRD) and selected area electron diffraction (SAED). The SAED pattern is in accordance with that of the simulation. Scanning and transmission electron microscopies (SEM and TEM) revealed the presence of different products consisting of nano-wires, nano-rods and tetra-pods controlled by Cd and S sources. High resolution TEM (HRTEM) showed that the products grew in [0 0 1] direction that was both parallel with and normal to their (1 0 0) and (0 0 2) planes, respectively. Raman spectra showed the same fundamental and overtone modes at 300 and 600 cm-1, respectively. © 2009 Elsevier B.V. All rights reserved. |
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Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
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Anukorn Phuruangrat Titipun Thongtem Somchai Thongtem |
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Anukorn Phuruangrat |
title |
Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents |
title_short |
Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents |
title_full |
Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents |
title_fullStr |
Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents |
title_full_unstemmed |
Effect of Cd and S sources on the morphologies of CdS synthesized by solvothermal reactions in mixed solvents |
title_sort |
effect of cd and s sources on the morphologies of cds synthesized by solvothermal reactions in mixed solvents |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=67349172558&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/59703 |
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