Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process

Li1-xNi1+xO2was prepared by the thermal-assisted precipitation process of LiOH • H2O and Ni(CH3COO)2• 4H2O at a pH of 6-13 followed by the high temperature calcination for a variety of prolonged times. Phases, morphologies and constituents were characterized using an x-ray diffractometer (XRD), a sc...

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Main Authors: Titipun Thongtem, Russamee Sitthikhankaew, Somchai Thongtem
Format: Journal
Published: 2018
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http://cmuir.cmu.ac.th/jspui/handle/6653943832/60257
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-602572018-09-10T03:40:12Z Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process Titipun Thongtem Russamee Sitthikhankaew Somchai Thongtem Chemistry Li1-xNi1+xO2was prepared by the thermal-assisted precipitation process of LiOH • H2O and Ni(CH3COO)2• 4H2O at a pH of 6-13 followed by the high temperature calcination for a variety of prolonged times. Phases, morphologies and constituents were characterized using an x-ray diffractometer (XRD), a scanning electron microscope (SEM), an energy dispersive x-ray (EDX) analyzer an atomic absorption spectrophotometer (AAS) and titration. Maximum [I(003)/I(104)] and minimum [I(006+102)/I(101)] intensity ratios were used to determine the preparation conditions. In addition, possible formation reactions of the precursors and calcined products were proposed. © 2008 MAIK Nauka. 2018-09-10T03:40:12Z 2018-09-10T03:40:12Z 2008-01-01 Journal 00360236 2-s2.0-43149085262 10.1134/S0036023608040050 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=43149085262&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60257
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Chemistry
spellingShingle Chemistry
Titipun Thongtem
Russamee Sitthikhankaew
Somchai Thongtem
Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process
description Li1-xNi1+xO2was prepared by the thermal-assisted precipitation process of LiOH • H2O and Ni(CH3COO)2• 4H2O at a pH of 6-13 followed by the high temperature calcination for a variety of prolonged times. Phases, morphologies and constituents were characterized using an x-ray diffractometer (XRD), a scanning electron microscope (SEM), an energy dispersive x-ray (EDX) analyzer an atomic absorption spectrophotometer (AAS) and titration. Maximum [I(003)/I(104)] and minimum [I(006+102)/I(101)] intensity ratios were used to determine the preparation conditions. In addition, possible formation reactions of the precursors and calcined products were proposed. © 2008 MAIK Nauka.
format Journal
author Titipun Thongtem
Russamee Sitthikhankaew
Somchai Thongtem
author_facet Titipun Thongtem
Russamee Sitthikhankaew
Somchai Thongtem
author_sort Titipun Thongtem
title Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process
title_short Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process
title_full Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process
title_fullStr Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process
title_full_unstemmed Characterization of Li<inf>1-x</inf>Ni<inf>1+x</inf>O<inf>2</inf>prepared by the thermal-assisted precipitation process
title_sort characterization of li<inf>1-x</inf>ni<inf>1+x</inf>o<inf>2</inf>prepared by the thermal-assisted precipitation process
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=43149085262&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/60257
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