Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals

Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals

PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electro...

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Main Authors: Titipun Thongtem, Sulawan Kaowphong, Somchai Thongtem
Format: Journal
Published: 2018
Subjects:
Materials Science
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=48349116217&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/60500
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-605002018-09-10T03:43:58Z Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals Titipun Thongtem Sulawan Kaowphong Somchai Thongtem Materials Science PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electron microscope (SEM), a transmission electron microscope (TEM), a selected area electron diffraction (SAED) technique and an energy dispersive X-ray (EDX) analyzer. In addition, a Raman spectrometer revealed the presence of the first and second overtone modes at 436 and 602 cm-1, respectively. Emission spectra of the products were detected at 412 nm using a photoluminescence (PL) spectrometer. © 2007 Elsevier Ltd and Techna Group S.r.l. 2018-09-10T03:43:58Z 2018-09-10T03:43:58Z 2008-09-01 Journal 02728842 2-s2.0-48349116217 10.1016/j.ceramint.2007.05.007 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=48349116217&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60500
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Materials Science
spellingShingle Materials Science
Titipun Thongtem
Sulawan Kaowphong
Somchai Thongtem
Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
description PbS crystals were hydrothermally synthesized using Pb(NO3)2, l-cysteine, and N-cetyl pyridinium chloride in solutions with different pH values at 140 °C. Flower-like, granular and truncated cubic PbS crystals composing of Pb and S were detected using an X-ray diffractometer (XRD), a scanning electron microscope (SEM), a transmission electron microscope (TEM), a selected area electron diffraction (SAED) technique and an energy dispersive X-ray (EDX) analyzer. In addition, a Raman spectrometer revealed the presence of the first and second overtone modes at 436 and 602 cm-1, respectively. Emission spectra of the products were detected at 412 nm using a photoluminescence (PL) spectrometer. © 2007 Elsevier Ltd and Techna Group S.r.l.
format Journal
author Titipun Thongtem
Sulawan Kaowphong
Somchai Thongtem
author_facet Titipun Thongtem
Sulawan Kaowphong
Somchai Thongtem
author_sort Titipun Thongtem
title Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_short Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_full Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_fullStr Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_full_unstemmed Biomolecule and surfactant-assisted hydrothermal synthesis of PbS crystals
title_sort biomolecule and surfactant-assisted hydrothermal synthesis of pbs crystals
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=48349116217&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/60500
_version_ 1681425447181615104

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