Effects of microwave heating on sonocatalyzed hydrothermal preparation of lead titanate nanopowders
Microwave heating has been applied in the sonocatalyzed hydrothermal preparation of tetragonal phase-pure lead titanate nanopowders with stoichiometric chemical composition. The effects and merits of microwave heating on the synthetic process and the obtained powder characteristics are demonstrated....
محفوظ في:
| المؤلفون الرئيسيون: | , , , |
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| التنسيق: | دورية |
| منشور في: |
2018
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| الموضوعات: | |
| الوصول للمادة أونلاين: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=46449117876&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60506 |
| الوسوم: |
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| المؤسسة: | Chiang Mai University |
| الملخص: | Microwave heating has been applied in the sonocatalyzed hydrothermal preparation of tetragonal phase-pure lead titanate nanopowders with stoichiometric chemical composition. The effects and merits of microwave heating on the synthetic process and the obtained powder characteristics are demonstrated. These include a reduction in reaction temperature to 95(± 5)°, which is the temperature of the water bath; a reduction of tetragonal distortion; and an improved regularity of the crystal habit. These non-thermal effects may be accounted for by a rapid mass transport induced by microwave electric field. © 2008 Elsevier B.V. All rights reserved. |
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