Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation

Nano- and micro-crystalline CdS was synthesized from cadmium [CdCl2·2H2O, Cd(NO3)2·4H2O, Cd(CH3COO)2·2H2O] and sulfur [CH3CSNH2, CH5N3S, CH6N4S] sources in ethylene glycol assisted by cyclic microwave radiation at different conditions. Phases (hcp and cubic) and morphologies (rose-shaped particles,...

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Main Authors:	Titipun Thongtem, Anukorn Phuruangrat, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=43449132094&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60524
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-60524
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spelling	th-cmuir.6653943832-605242018-09-10T03:48:28Z Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem Materials Science Physics and Astronomy Nano- and micro-crystalline CdS was synthesized from cadmium [CdCl2·2H2O, Cd(NO3)2·4H2O, Cd(CH3COO)2·2H2O] and sulfur [CH3CSNH2, CH5N3S, CH6N4S] sources in ethylene glycol assisted by cyclic microwave radiation at different conditions. Phases (hcp and cubic) and morphologies (rose-shaped particles, spikes in cluster, cauliflowers, and nano-particles in cluster) were detected using XRD, SAED, TEM, and SEM, and influenced by Cd and S sources. The crystalline products are aligned in a systematic array and analyzed by HRTEM. A Raman spectrometer revealed the presence of fundamental and overtone modes at 298 and 597 cm-1, respectively. Exposure times and microwave powers also play a role in the crystallinity and size of the products. © 2007 Elsevier Ltd. All rights reserved. 2018-09-10T03:44:17Z 2018-09-10T03:44:17Z 2008-05-01 Journal 00223697 2-s2.0-43449132094 10.1016/j.jpcs.2007.10.036 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=43449132094&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60524
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Materials Science Physics and Astronomy
spellingShingle	Materials Science Physics and Astronomy Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation
description	Nano- and micro-crystalline CdS was synthesized from cadmium [CdCl2·2H2O, Cd(NO3)2·4H2O, Cd(CH3COO)2·2H2O] and sulfur [CH3CSNH2, CH5N3S, CH6N4S] sources in ethylene glycol assisted by cyclic microwave radiation at different conditions. Phases (hcp and cubic) and morphologies (rose-shaped particles, spikes in cluster, cauliflowers, and nano-particles in cluster) were detected using XRD, SAED, TEM, and SEM, and influenced by Cd and S sources. The crystalline products are aligned in a systematic array and analyzed by HRTEM. A Raman spectrometer revealed the presence of fundamental and overtone modes at 298 and 597 cm-1, respectively. Exposure times and microwave powers also play a role in the crystallinity and size of the products. © 2007 Elsevier Ltd. All rights reserved.
format	Journal
author	Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem
author_facet	Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem
author_sort	Titipun Thongtem
title	Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation
title_short	Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation
title_full	Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation
title_fullStr	Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation
title_full_unstemmed	Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation
title_sort	characterization of nano- and micro-crystalline cds synthesized using cyclic microwave radiation
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=43449132094&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/60524
_version_	1681425451630723072

Characterization of nano- and micro-crystalline CdS synthesized using cyclic microwave radiation

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