Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA

A simple spectrophotometric flow injection (FI) procedure for the determination of Cr(III) using ethylenediaminetetraacetic acid (EDTA) was developed. An FI system with a column packed with Amberlite IR-120(H) was employed for sample pretreatment. This leads to the possibility of a single standard c...

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Main Authors: Lapanantnoppakhun S., Kasuwas S., Ganranoo L., Jakmunee J., Grudpan K.
Format: Article
Language:English
Published: 2014
Online Access:http://www.ncbi.nlm.nih.gov/pubmed/3502482
http://cmuir.cmu.ac.th/handle/6653943832/6098
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Institution: Chiang Mai University
Language: English
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spelling th-cmuir.6653943832-60982014-08-30T03:23:50Z Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA Lapanantnoppakhun S. Kasuwas S. Ganranoo L. Jakmunee J. Grudpan K. A simple spectrophotometric flow injection (FI) procedure for the determination of Cr(III) using ethylenediaminetetraacetic acid (EDTA) was developed. An FI system with a column packed with Amberlite IR-120(H) was employed for sample pretreatment. This leads to the possibility of a single standard calibration. A linear calibration in a range of 10-27 microg Cr(III) was obtained with a detection limit of 1 microg Cr(III) and RSD of 2% (18 microg Cr(III), n=12). The proposed procedure was applied for determination of Cr(III) in leachate and dietary supplement samples. The results agreed with those obtained by the standard methods. 2014-08-30T03:23:50Z 2014-08-30T03:23:50Z 2006 Journal Article 0910-6340 16429793 http://www.ncbi.nlm.nih.gov/pubmed/3502482 http://cmuir.cmu.ac.th/handle/6653943832/6098 eng
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
language English
description A simple spectrophotometric flow injection (FI) procedure for the determination of Cr(III) using ethylenediaminetetraacetic acid (EDTA) was developed. An FI system with a column packed with Amberlite IR-120(H) was employed for sample pretreatment. This leads to the possibility of a single standard calibration. A linear calibration in a range of 10-27 microg Cr(III) was obtained with a detection limit of 1 microg Cr(III) and RSD of 2% (18 microg Cr(III), n=12). The proposed procedure was applied for determination of Cr(III) in leachate and dietary supplement samples. The results agreed with those obtained by the standard methods.
format Article
author Lapanantnoppakhun S.
Kasuwas S.
Ganranoo L.
Jakmunee J.
Grudpan K.
spellingShingle Lapanantnoppakhun S.
Kasuwas S.
Ganranoo L.
Jakmunee J.
Grudpan K.
Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA
author_facet Lapanantnoppakhun S.
Kasuwas S.
Ganranoo L.
Jakmunee J.
Grudpan K.
author_sort Lapanantnoppakhun S.
title Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA
title_short Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA
title_full Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA
title_fullStr Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA
title_full_unstemmed Simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(III) using EDTA
title_sort simple spectrophotometric flow injection system with an in-valve minicolumn for enhancement during the determination of chromium(iii) using edta
publishDate 2014
url http://www.ncbi.nlm.nih.gov/pubmed/3502482
http://cmuir.cmu.ac.th/handle/6653943832/6098
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