Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling
Effect of calcination conditions on phase formation and particle size of lead zirconate (PbZrO3) powders synthesized by a solid-state reaction with different vibro-milling times was investigated. A combination of the milling time and calcination conditions was found to have a pronounced effect on bo...
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th-cmuir.6653943832-610722018-09-10T04:06:01Z Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling O. Khamman T. Sarakonsri A. Rujiwatra Y. Laosiritaworn R. Yimnirun S. Ananta Engineering Materials Science Effect of calcination conditions on phase formation and particle size of lead zirconate (PbZrO3) powders synthesized by a solid-state reaction with different vibro-milling times was investigated. A combination of the milling time and calcination conditions was found to have a pronounced effect on both the phase formation and particle size of the calcined PbZrO3powders. The calcination temperature for the formation of single-phase perovskite lead zirconate was lower when longer milling times were applied. The optimal combination of the milling time and calcination condition for the production of the smallest nanosized (∼28 nm) high purity PbZrO3powders is 35 h and 750 °C for 4 h with heating/cooling rates of 30 °C/min, respectively. © 2007 Springer Science+Business Media, LLC. 2018-09-10T04:03:47Z 2018-09-10T04:03:47Z 2007-10-01 Journal 15734803 00222461 2-s2.0-34547753569 10.1007/s10853-007-1776-6 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34547753569&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61072 |
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Engineering Materials Science O. Khamman T. Sarakonsri A. Rujiwatra Y. Laosiritaworn R. Yimnirun S. Ananta Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling |
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Effect of calcination conditions on phase formation and particle size of lead zirconate (PbZrO3) powders synthesized by a solid-state reaction with different vibro-milling times was investigated. A combination of the milling time and calcination conditions was found to have a pronounced effect on both the phase formation and particle size of the calcined PbZrO3powders. The calcination temperature for the formation of single-phase perovskite lead zirconate was lower when longer milling times were applied. The optimal combination of the milling time and calcination condition for the production of the smallest nanosized (∼28 nm) high purity PbZrO3powders is 35 h and 750 °C for 4 h with heating/cooling rates of 30 °C/min, respectively. © 2007 Springer Science+Business Media, LLC. |
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O. Khamman T. Sarakonsri A. Rujiwatra Y. Laosiritaworn R. Yimnirun S. Ananta |
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O. Khamman T. Sarakonsri A. Rujiwatra Y. Laosiritaworn R. Yimnirun S. Ananta |
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O. Khamman |
title |
Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling |
title_short |
Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling |
title_full |
Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling |
title_fullStr |
Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling |
title_full_unstemmed |
Effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling |
title_sort |
effects of milling time and calcination condition on phase formation and particle size of lead zirconate nanopowders prepared by vibro-milling |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34547753569&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61072 |
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