Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent

LiNiVO4was prepared from Li2CO3, Ni(CH3COO)2·4H2O and NH4VO3using tartaric acid as a complexing agent with 1:1-1:4 mole ratios of metals:tartaric acid and subsequent calcination at 350-700 °C for 6-12 h. Inverse spinel LiNiVO4was detected using XRD. FTIR and Raman analyses revealed the presence of s...

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Main Authors:	Titipun Thongtem, Sulawan Kaowphong, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Materials Science
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34548822402&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61155
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-61155
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spelling	th-cmuir.6653943832-611552018-09-10T04:05:42Z Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent Titipun Thongtem Sulawan Kaowphong Somchai Thongtem Materials Science LiNiVO4was prepared from Li2CO3, Ni(CH3COO)2·4H2O and NH4VO3using tartaric acid as a complexing agent with 1:1-1:4 mole ratios of metals:tartaric acid and subsequent calcination at 350-700 °C for 6-12 h. Inverse spinel LiNiVO4was detected using XRD. FTIR and Raman analyses revealed the presence of stretching band of VO4tetrahedrons. Only Ni, V and O were detected by EDX. The 1:4 mole ratio for the product with 450 °C calcination for 6 h analyzed by SEM, TEM and electron diffraction (ED) composes of LiNiVO4nano-powder with 10-30 nm in diameter. © 2006 Elsevier Ltd and Techna Group S.r.l. 2018-09-10T04:05:42Z 2018-09-10T04:05:42Z 2007-12-01 Journal 02728842 2-s2.0-34548822402 10.1016/j.ceramint.2006.05.005 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34548822402&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61155
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Materials Science
spellingShingle	Materials Science Titipun Thongtem Sulawan Kaowphong Somchai Thongtem Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent
description	LiNiVO4was prepared from Li2CO3, Ni(CH3COO)2·4H2O and NH4VO3using tartaric acid as a complexing agent with 1:1-1:4 mole ratios of metals:tartaric acid and subsequent calcination at 350-700 °C for 6-12 h. Inverse spinel LiNiVO4was detected using XRD. FTIR and Raman analyses revealed the presence of stretching band of VO4tetrahedrons. Only Ni, V and O were detected by EDX. The 1:4 mole ratio for the product with 450 °C calcination for 6 h analyzed by SEM, TEM and electron diffraction (ED) composes of LiNiVO4nano-powder with 10-30 nm in diameter. © 2006 Elsevier Ltd and Techna Group S.r.l.
format	Journal
author	Titipun Thongtem Sulawan Kaowphong Somchai Thongtem
author_facet	Titipun Thongtem Sulawan Kaowphong Somchai Thongtem
author_sort	Titipun Thongtem
title	Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent
title_short	Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent
title_full	Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent
title_fullStr	Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent
title_full_unstemmed	Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent
title_sort	preparation of linivo4 nano-powder using tartaric acid as a complexing agent
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34548822402&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61155
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Preparation of LiNiVO4 nano-powder using tartaric acid as a complexing agent

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