A two-stage solid-state reaction to lead zirconate titanate powders

An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite ph...

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Main Authors:	Wanwilai Chaisan, Orawan Khamman, Rattikorn Yimnirun, Supon Ananta
Format:	Journal
Published:	2018
Subjects:	Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-61161
record_format	dspace
spelling	th-cmuir.6653943832-611612018-09-10T04:09:56Z A two-stage solid-state reaction to lead zirconate titanate powders Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta Materials Science Physics and Astronomy An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3and PbTiO3phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase. 2018-09-10T04:05:45Z 2018-09-10T04:05:45Z 2007-12-01 Journal 15635112 00150193 2-s2.0-75449085131 10.1080/00150190701512763 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Materials Science Physics and Astronomy
spellingShingle	Materials Science Physics and Astronomy Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta A two-stage solid-state reaction to lead zirconate titanate powders
description	An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3and PbTiO3phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase.
format	Journal
author	Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta
author_facet	Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta
author_sort	Wanwilai Chaisan
title	A two-stage solid-state reaction to lead zirconate titanate powders
title_short	A two-stage solid-state reaction to lead zirconate titanate powders
title_full	A two-stage solid-state reaction to lead zirconate titanate powders
title_fullStr	A two-stage solid-state reaction to lead zirconate titanate powders
title_full_unstemmed	A two-stage solid-state reaction to lead zirconate titanate powders
title_sort	two-stage solid-state reaction to lead zirconate titanate powders
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161
_version_	1681425569213841408

A two-stage solid-state reaction to lead zirconate titanate powders

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