A two-stage solid-state reaction to lead zirconate titanate powders
An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite ph...
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th-cmuir.6653943832-611612018-09-10T04:09:56Z A two-stage solid-state reaction to lead zirconate titanate powders Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta Materials Science Physics and Astronomy An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3and PbTiO3phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase. 2018-09-10T04:05:45Z 2018-09-10T04:05:45Z 2007-12-01 Journal 15635112 00150193 2-s2.0-75449085131 10.1080/00150190701512763 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161 |
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Materials Science Physics and Astronomy Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta A two-stage solid-state reaction to lead zirconate titanate powders |
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An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3and PbTiO3phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase. |
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Journal |
author |
Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta |
author_facet |
Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta |
author_sort |
Wanwilai Chaisan |
title |
A two-stage solid-state reaction to lead zirconate titanate powders |
title_short |
A two-stage solid-state reaction to lead zirconate titanate powders |
title_full |
A two-stage solid-state reaction to lead zirconate titanate powders |
title_fullStr |
A two-stage solid-state reaction to lead zirconate titanate powders |
title_full_unstemmed |
A two-stage solid-state reaction to lead zirconate titanate powders |
title_sort |
two-stage solid-state reaction to lead zirconate titanate powders |
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2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161 |
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