A two-stage solid-state reaction to lead zirconate titanate powders

An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite ph...

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Main Authors: Wanwilai Chaisan, Orawan Khamman, Rattikorn Yimnirun, Supon Ananta
Format: Journal
Published: 2018
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Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-611612018-09-10T04:09:56Z A two-stage solid-state reaction to lead zirconate titanate powders Wanwilai Chaisan Orawan Khamman Rattikorn Yimnirun Supon Ananta Materials Science Physics and Astronomy An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3and PbTiO3phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase. 2018-09-10T04:05:45Z 2018-09-10T04:05:45Z 2007-12-01 Journal 15635112 00150193 2-s2.0-75449085131 10.1080/00150190701512763 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Materials Science
Physics and Astronomy
spellingShingle Materials Science
Physics and Astronomy
Wanwilai Chaisan
Orawan Khamman
Rattikorn Yimnirun
Supon Ananta
A two-stage solid-state reaction to lead zirconate titanate powders
description An approach to synthesize lead zirconate titanate (PZT) powders with a modified two-stage mixed oxide synthetic route has been developed. To ensure a single-phase perovskite formation, an intermediate phase of lead zirconate (PbZrO3) was employed as starting precursor. The formation of perovskite phase in the calcined powders has been investigated as a function of calcination temperature. It has been found that the perovskite PbZrO3and PbTiO3phases tend to form together with PZT, with the latter appearing in both tetragonal and rhombohedral phases, depending on calcination temperatures. It is seen that optimization of calcination can lead to 100% yield of PZT phase.
format Journal
author Wanwilai Chaisan
Orawan Khamman
Rattikorn Yimnirun
Supon Ananta
author_facet Wanwilai Chaisan
Orawan Khamman
Rattikorn Yimnirun
Supon Ananta
author_sort Wanwilai Chaisan
title A two-stage solid-state reaction to lead zirconate titanate powders
title_short A two-stage solid-state reaction to lead zirconate titanate powders
title_full A two-stage solid-state reaction to lead zirconate titanate powders
title_fullStr A two-stage solid-state reaction to lead zirconate titanate powders
title_full_unstemmed A two-stage solid-state reaction to lead zirconate titanate powders
title_sort two-stage solid-state reaction to lead zirconate titanate powders
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=75449085131&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/61161
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