Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction

Zirconium titanate (ZrTiO4; ZT) powders have been prepared by using a solid-state reaction combined with a vibro-milling technique. The effects of calcination temperature, dwell time and heating/cooling rates on phase formation and morphology of the powders were examined. The calcination temperature...

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Main Authors:	Anurak Prasatkhetragarn, Rattikorn Yimnirun, Supon Ananta
Format:	Journal
Published:	2018
Subjects:	Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=62949238329&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61165
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Institution:	Chiang Mai University

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spelling	th-cmuir.6653943832-611652018-09-10T04:09:58Z Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction Anurak Prasatkhetragarn Rattikorn Yimnirun Supon Ananta Materials Science Physics and Astronomy Zirconium titanate (ZrTiO4; ZT) powders have been prepared by using a solid-state reaction combined with a vibro-milling technique. The effects of calcination temperature, dwell time and heating/cooling rates on phase formation and morphology of the powders were examined. The calcination temperature and dwell time have been found to show a pronounced effect on the phase formation of the calcined zirconium titanate powders. Additionally, the minor phase of unreacted TiO2tends to form together with ZrTiO4, depending on calcination conditions. It is seen that optimization of calcination conditions can lead to 100% yield of an orthorhombic ZrTiO4. 2018-09-10T04:05:47Z 2018-09-10T04:05:47Z 2007-12-01 Journal 15635112 00150193 2-s2.0-62949238329 10.1080/00150190701512367 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=62949238329&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61165
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Materials Science Physics and Astronomy
spellingShingle	Materials Science Physics and Astronomy Anurak Prasatkhetragarn Rattikorn Yimnirun Supon Ananta Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction
description	Zirconium titanate (ZrTiO4; ZT) powders have been prepared by using a solid-state reaction combined with a vibro-milling technique. The effects of calcination temperature, dwell time and heating/cooling rates on phase formation and morphology of the powders were examined. The calcination temperature and dwell time have been found to show a pronounced effect on the phase formation of the calcined zirconium titanate powders. Additionally, the minor phase of unreacted TiO2tends to form together with ZrTiO4, depending on calcination conditions. It is seen that optimization of calcination conditions can lead to 100% yield of an orthorhombic ZrTiO4.
format	Journal
author	Anurak Prasatkhetragarn Rattikorn Yimnirun Supon Ananta
author_facet	Anurak Prasatkhetragarn Rattikorn Yimnirun Supon Ananta
author_sort	Anurak Prasatkhetragarn
title	Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction
title_short	Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction
title_full	Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction
title_fullStr	Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction
title_full_unstemmed	Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction
title_sort	effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=62949238329&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61165
_version_	1681425569962524672

Effect of calcination condition on phase formation of zirconium titanate powders synthesized by the solid-state reaction

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