Barium titanate nanopowders prepared from the modified oxalate co-precipitation method
Barium titanate nanopowders were prepared from the modified oxalate co-precipitation method. Barium chloride dihydrate and potassium titanyl oxalate dihydrate were used as the starting precursors with the mole ratio of Ba:Ti as 1:1. Barium titanyl oxalate complex powders were obtained after adjustin...
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| Main Authors: | , , |
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| Format: | Book Series |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=38349107978&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61169 |
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| Institution: | Chiang Mai University |
| Summary: | Barium titanate nanopowders were prepared from the modified oxalate co-precipitation method. Barium chloride dihydrate and potassium titanyl oxalate dihydrate were used as the starting precursors with the mole ratio of Ba:Ti as 1:1. Barium titanyl oxalate complex powders were obtained after adjusting the final of pH of the solution to 1. The precipitates were filtered, washed and dried at 100 °C for 5h. The precipitate powders were calcined at 400-700 °C for 2h. The phase transition was studied by X-ray diffractometry (XRD). Cubic structure of barium titanate was obtained after calcinations at 700 °C for 2h. The morphology and chemical composition were investigated by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDXS). The range of particle size was 50-100 nm with irregular in shape. The elemental composition of barium, titanium and oxygen showed the characteristic X-ray energy values. |
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