Sonocatalyzed hydrothermal preparation of lead titanate nanopowders
Nanoparticles of perovskite lead titanate, PbTiO3, were successfully prepared in a stoichiometric proportion at conspicuously low temperature and short reaction time of only 130 °C and 3.5 h. The employment of ultrasonic treatment prior to hydrothermal reaction, or so-called "sonocatalyzed hydr...
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| Main Authors: | , , , |
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| Format: | Journal |
| Published: |
2018
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| Subjects: | |
| Online Access: | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34548029987&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61176 |
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| Institution: | Chiang Mai University |
| Summary: | Nanoparticles of perovskite lead titanate, PbTiO3, were successfully prepared in a stoichiometric proportion at conspicuously low temperature and short reaction time of only 130 °C and 3.5 h. The employment of ultrasonic treatment prior to hydrothermal reaction, or so-called "sonocatalyzed hydrothermal reaction", was examined in detail. Roles of ultrasonic wave both as a catalyst to lower the hydrothermal reaction temperature affording the phase-pure PbTiO3and as an external influence to provide better size homogeneity were discussed. © 2007 Elsevier B.V. All rights reserved. |
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