Malic acid complex method for preparation of LiNiVO4 nano-crystallites
LiNiVO4nano-crystallites were prepared by the polymerized complex method using Li2CO3, Ni(CH3COO)2•4H2O and NH4VO3as starting reagents and malic acid as a complexing agent. With the subsequent calcination at 450°C, the powder analyzed by XRD, FTIR, Raman, electron diffraction, SEM and TEM techniques...
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th-cmuir.6653943832-611942018-09-10T04:10:34Z Malic acid complex method for preparation of LiNiVO4 nano-crystallites Titipun Thongtem Sulawan Kaowphong Somchai Thongtem Materials Science Physics and Astronomy LiNiVO4nano-crystallites were prepared by the polymerized complex method using Li2CO3, Ni(CH3COO)2•4H2O and NH4VO3as starting reagents and malic acid as a complexing agent. With the subsequent calcination at 450°C, the powder analyzed by XRD, FTIR, Raman, electron diffraction, SEM and TEM techniques was found to be inverse spinel LiNiVO4with ~20nm in diameter. TGA shows continuous weight loss at 40-450°C due to the evaporation and decomposition processes. Above 450°C, weight percent tended to be constant. In addition, formation mechanism of the purified LiNiVO4was proposed to relate with the experimental results. © Springer Science+Business Media, LLC 2007. 2018-09-10T04:06:22Z 2018-09-10T04:06:22Z 2007-06-01 Journal 15734803 00222461 2-s2.0-34249816830 10.1007/s10853-006-0402-3 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34249816830&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61194 |
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Materials Science Physics and Astronomy |
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Materials Science Physics and Astronomy Titipun Thongtem Sulawan Kaowphong Somchai Thongtem Malic acid complex method for preparation of LiNiVO4 nano-crystallites |
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LiNiVO4nano-crystallites were prepared by the polymerized complex method using Li2CO3, Ni(CH3COO)2•4H2O and NH4VO3as starting reagents and malic acid as a complexing agent. With the subsequent calcination at 450°C, the powder analyzed by XRD, FTIR, Raman, electron diffraction, SEM and TEM techniques was found to be inverse spinel LiNiVO4with ~20nm in diameter. TGA shows continuous weight loss at 40-450°C due to the evaporation and decomposition processes. Above 450°C, weight percent tended to be constant. In addition, formation mechanism of the purified LiNiVO4was proposed to relate with the experimental results. © Springer Science+Business Media, LLC 2007. |
| format |
Journal |
| author |
Titipun Thongtem Sulawan Kaowphong Somchai Thongtem |
| author_facet |
Titipun Thongtem Sulawan Kaowphong Somchai Thongtem |
| author_sort |
Titipun Thongtem |
| title |
Malic acid complex method for preparation of LiNiVO4 nano-crystallites |
| title_short |
Malic acid complex method for preparation of LiNiVO4 nano-crystallites |
| title_full |
Malic acid complex method for preparation of LiNiVO4 nano-crystallites |
| title_fullStr |
Malic acid complex method for preparation of LiNiVO4 nano-crystallites |
| title_full_unstemmed |
Malic acid complex method for preparation of LiNiVO4 nano-crystallites |
| title_sort |
malic acid complex method for preparation of linivo4 nano-crystallites |
| publishDate |
2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34249816830&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61194 |
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