Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders
A perovskite phase of lead zirconate, PbZrO3, nanopowder was synthesized by a solid-state reaction via a rapid vibro-milling technique. The effect of milling time on the phase formation and particle size of PbZrO3 powder was investigated. Powder samples were characterized using TG-DTA, XRD, SEM and...
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th-cmuir.6653943832-611962018-09-10T04:06:25Z Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders O. Khamman W. Chaisan R. Yimnirun S. Ananta Materials Science A perovskite phase of lead zirconate, PbZrO3, nanopowder was synthesized by a solid-state reaction via a rapid vibro-milling technique. The effect of milling time on the phase formation and particle size of PbZrO3 powder was investigated. Powder samples were characterized using TG-DTA, XRD, SEM and laser diffraction techniques. It was found that an average particle size of 50 nm was achieved at 25 h of vibro-milling after which a higher degree of particle agglomeration was observed upon continuation of milling to 35 h. In addition, by employing an appropriate choice of milling time, a narrow particle size distribution curve was also observed. © 2006 Elsevier B.V. All rights reserved. 2018-09-10T04:06:25Z 2018-09-10T04:06:25Z 2007-05-01 Journal 0167577X 2-s2.0-34247124093 10.1016/j.matlet.2006.10.063 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34247124093&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61196 |
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Materials Science O. Khamman W. Chaisan R. Yimnirun S. Ananta Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders |
| description |
A perovskite phase of lead zirconate, PbZrO3, nanopowder was synthesized by a solid-state reaction via a rapid vibro-milling technique. The effect of milling time on the phase formation and particle size of PbZrO3 powder was investigated. Powder samples were characterized using TG-DTA, XRD, SEM and laser diffraction techniques. It was found that an average particle size of 50 nm was achieved at 25 h of vibro-milling after which a higher degree of particle agglomeration was observed upon continuation of milling to 35 h. In addition, by employing an appropriate choice of milling time, a narrow particle size distribution curve was also observed. © 2006 Elsevier B.V. All rights reserved. |
| format |
Journal |
| author |
O. Khamman W. Chaisan R. Yimnirun S. Ananta |
| author_facet |
O. Khamman W. Chaisan R. Yimnirun S. Ananta |
| author_sort |
O. Khamman |
| title |
Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders |
| title_short |
Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders |
| title_full |
Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders |
| title_fullStr |
Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders |
| title_full_unstemmed |
Effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders |
| title_sort |
effect of vibro-milling time on phase formation and particle size of lead zirconate nanopowders |
| publishDate |
2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=34247124093&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61196 |
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