The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications
Cu0.5Ag1.5InSe3 compound which is used as a thermoelectric material was successfully synthesized by a simple solution route. The metal ions were reduced simultaneously under alkaline conditions by NaBH4. The types of solvent, reaction temperature, indium precursors, and reaction time were studied as...
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th-cmuir.6653943832-61432014-08-30T03:23:53Z The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications Chansaenpak K. Sarakonsri T. Cu0.5Ag1.5InSe3 compound which is used as a thermoelectric material was successfully synthesized by a simple solution route. The metal ions were reduced simultaneously under alkaline conditions by NaBH4. The types of solvent, reaction temperature, indium precursors, and reaction time were studied as the parameters of the synthesis method. The prepared powders were investigated by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and energy dispersive X-ray spectroscopy (EDS). The results show that the reaction temperature is the main factor affecting Cu0.5Ag1.5InSe3 formation. Finally, suitable conditions to prepare Cu0.5Ag1.5InSe3 particles were ethylene glycol as a solvent, 200 degree Celsius as a reaction temperature, indium nitrate as an indium precursor, and 72 h as a reaction time. 2014-08-30T03:23:53Z 2014-08-30T03:23:53Z 2010 Article 12299162 http://www.scopus.com/inward/record.url?eid=2-s2.0-79251489136&partnerID=40&md5=986477c36fbf53d17cf68d14c91ac943 http://cmuir.cmu.ac.th/handle/6653943832/6143 English |
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Cu0.5Ag1.5InSe3 compound which is used as a thermoelectric material was successfully synthesized by a simple solution route. The metal ions were reduced simultaneously under alkaline conditions by NaBH4. The types of solvent, reaction temperature, indium precursors, and reaction time were studied as the parameters of the synthesis method. The prepared powders were investigated by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and energy dispersive X-ray spectroscopy (EDS). The results show that the reaction temperature is the main factor affecting Cu0.5Ag1.5InSe3 formation. Finally, suitable conditions to prepare Cu0.5Ag1.5InSe3 particles were ethylene glycol as a solvent, 200 degree Celsius as a reaction temperature, indium nitrate as an indium precursor, and 72 h as a reaction time. |
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Article |
author |
Chansaenpak K. Sarakonsri T. |
spellingShingle |
Chansaenpak K. Sarakonsri T. The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications |
author_facet |
Chansaenpak K. Sarakonsri T. |
author_sort |
Chansaenpak K. |
title |
The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications |
title_short |
The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications |
title_full |
The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications |
title_fullStr |
The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications |
title_full_unstemmed |
The solution route synthesis of the Cu0.5Ag1.5InSe3 compound for thermoelectric applications |
title_sort |
solution route synthesis of the cu0.5ag1.5inse3 compound for thermoelectric applications |
publishDate |
2014 |
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http://www.scopus.com/inward/record.url?eid=2-s2.0-79251489136&partnerID=40&md5=986477c36fbf53d17cf68d14c91ac943 http://cmuir.cmu.ac.th/handle/6653943832/6143 |
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