One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate

Phase-pure and stoichiometric lead zirconate powders consisting of submicro- to micrometer-sized particles were successfully synthesized via a simple, one-pot hydrothermal technique at moderate temperatures and short reaction times. High concentration of potassium hydroxide mineralizer was necessary...

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Main Authors:	Apinpus Rujiwatra, Saowalak Tapala, Sanchai Luachan, Orawan Khamman, Supon Ananta
Format:	Journal
Published:	2018
Subjects:	Engineering Materials Science Physics and Astronomy
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33746368694&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61669
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-61669
record_format	dspace
spelling	th-cmuir.6653943832-616692018-09-11T09:01:53Z One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate Apinpus Rujiwatra Saowalak Tapala Sanchai Luachan Orawan Khamman Supon Ananta Engineering Materials Science Physics and Astronomy Phase-pure and stoichiometric lead zirconate powders consisting of submicro- to micrometer-sized particles were successfully synthesized via a simple, one-pot hydrothermal technique at moderate temperatures and short reaction times. High concentration of potassium hydroxide mineralizer was necessary in the formation of well-crystalline lead zirconate. The type of zirconium precursor, reaction temperature and time showed apparent influences over particle shape, size and distribution. Transmission electron microscope was used to confirm the crystallographic setting of the prepared lead zirconate. © 2006 Elsevier B.V. All rights reserved. 2018-09-11T08:56:50Z 2018-09-11T08:56:50Z 2006-10-01 Journal 0167577X 2-s2.0-33746368694 10.1016/j.matlet.2006.02.010 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33746368694&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61669
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Engineering Materials Science Physics and Astronomy
spellingShingle	Engineering Materials Science Physics and Astronomy Apinpus Rujiwatra Saowalak Tapala Sanchai Luachan Orawan Khamman Supon Ananta One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
description	Phase-pure and stoichiometric lead zirconate powders consisting of submicro- to micrometer-sized particles were successfully synthesized via a simple, one-pot hydrothermal technique at moderate temperatures and short reaction times. High concentration of potassium hydroxide mineralizer was necessary in the formation of well-crystalline lead zirconate. The type of zirconium precursor, reaction temperature and time showed apparent influences over particle shape, size and distribution. Transmission electron microscope was used to confirm the crystallographic setting of the prepared lead zirconate. © 2006 Elsevier B.V. All rights reserved.
format	Journal
author	Apinpus Rujiwatra Saowalak Tapala Sanchai Luachan Orawan Khamman Supon Ananta
author_facet	Apinpus Rujiwatra Saowalak Tapala Sanchai Luachan Orawan Khamman Supon Ananta
author_sort	Apinpus Rujiwatra
title	One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
title_short	One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
title_full	One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
title_fullStr	One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
title_full_unstemmed	One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
title_sort	one-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33746368694&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61669
_version_	1681425663715704832

One-pot hydrothermal synthesis of highly dispersed, phase-pure and stoichiometric lead zirconate

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