Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders
A perovskite-like phase of lead titanate, PbTiO3, nanopowder was synthesized by a solid-state reaction via a rapid vibro-milling technique. The effect of milling time on the phase formation and particle size of PbTiO3powder was investigated. Powder samples were characterized using TG-DTA, XRD, SEM a...
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th-cmuir.6653943832-616842018-09-11T09:02:16Z Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders R. Wongmaneerung R. Yimnirun S. Ananta Engineering Materials Science Physics and Astronomy A perovskite-like phase of lead titanate, PbTiO3, nanopowder was synthesized by a solid-state reaction via a rapid vibro-milling technique. The effect of milling time on the phase formation and particle size of PbTiO3powder was investigated. Powder samples were characterized using TG-DTA, XRD, SEM and laser diffraction techniques. It was found that an average particle size of 17 nm was achieved at 25 h of vibro-milling after which a higher degree of particle agglomeration was observed on continuation of milling to 35 h. In addition, by employing an appropriate choice of the milling time, a narrow particle size distribution curve was also observed. © 2005 Elsevier B.V. All rights reserved. 2018-09-11T08:57:02Z 2018-09-11T08:57:02Z 2006-06-01 Journal 0167577X 2-s2.0-33644870261 10.1016/j.matlet.2005.11.043 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33644870261&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61684 |
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Engineering Materials Science Physics and Astronomy |
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Engineering Materials Science Physics and Astronomy R. Wongmaneerung R. Yimnirun S. Ananta Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders |
| description |
A perovskite-like phase of lead titanate, PbTiO3, nanopowder was synthesized by a solid-state reaction via a rapid vibro-milling technique. The effect of milling time on the phase formation and particle size of PbTiO3powder was investigated. Powder samples were characterized using TG-DTA, XRD, SEM and laser diffraction techniques. It was found that an average particle size of 17 nm was achieved at 25 h of vibro-milling after which a higher degree of particle agglomeration was observed on continuation of milling to 35 h. In addition, by employing an appropriate choice of the milling time, a narrow particle size distribution curve was also observed. © 2005 Elsevier B.V. All rights reserved. |
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Journal |
| author |
R. Wongmaneerung R. Yimnirun S. Ananta |
| author_facet |
R. Wongmaneerung R. Yimnirun S. Ananta |
| author_sort |
R. Wongmaneerung |
| title |
Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders |
| title_short |
Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders |
| title_full |
Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders |
| title_fullStr |
Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders |
| title_full_unstemmed |
Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders |
| title_sort |
effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders |
| publishDate |
2018 |
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https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33644870261&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61684 |
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