Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction

LiOH·H2O, Co(NO3)2·6H2O and NH4VO3were used to prepare nano-crystalline LiCoVO4by 150 °C solvothermal reaction in isopropanol for 10-360 h and subsequent calcination at 300-500 °C for 6 h. XRD, TEM and selected area electron diffraction (SAED) revealed the presence of nano-crystalline LiCoVO4with in...

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Main Authors:	Titipun Thongtem, Anukorn Phuruangrat, Somchai Thongtem
Format:	Journal
Published:	2018
Subjects:	Materials Science
Online Access:	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33750284297&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61730
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Institution:	Chiang Mai University

id	th-cmuir.6653943832-61730
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spelling	th-cmuir.6653943832-617302018-09-11T08:58:07Z Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem Materials Science LiOH·H2O, Co(NO3)2·6H2O and NH4VO3were used to prepare nano-crystalline LiCoVO4by 150 °C solvothermal reaction in isopropanol for 10-360 h and subsequent calcination at 300-500 °C for 6 h. XRD, TEM and selected area electron diffraction (SAED) revealed the presence of nano-crystalline LiCoVO4with inverse spinel structure. The V-O stretching vibration modes of VO4tetrahedrons were detected by FTIR over the range 617-835 cm- 1and by Raman spectrometer at 805.7 and 783.1 cm- 1. Co, V and O were detected by EDX. TGA of solvothermal products shows weight loss due to the evaporation and decomposition processes at 40-648 °C. © 2006 Elsevier B.V. All rights reserved. 2018-09-11T08:58:07Z 2018-09-11T08:58:07Z 2006-12-01 Journal 0167577X 2-s2.0-33750284297 10.1016/j.matlet.2006.03.111 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33750284297&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61730
institution	Chiang Mai University
building	Chiang Mai University Library
country	Thailand
collection	CMU Intellectual Repository
topic	Materials Science
spellingShingle	Materials Science Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction
description	LiOH·H2O, Co(NO3)2·6H2O and NH4VO3were used to prepare nano-crystalline LiCoVO4by 150 °C solvothermal reaction in isopropanol for 10-360 h and subsequent calcination at 300-500 °C for 6 h. XRD, TEM and selected area electron diffraction (SAED) revealed the presence of nano-crystalline LiCoVO4with inverse spinel structure. The V-O stretching vibration modes of VO4tetrahedrons were detected by FTIR over the range 617-835 cm- 1and by Raman spectrometer at 805.7 and 783.1 cm- 1. Co, V and O were detected by EDX. TGA of solvothermal products shows weight loss due to the evaporation and decomposition processes at 40-648 °C. © 2006 Elsevier B.V. All rights reserved.
format	Journal
author	Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem
author_facet	Titipun Thongtem Anukorn Phuruangrat Somchai Thongtem
author_sort	Titipun Thongtem
title	Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction
title_short	Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction
title_full	Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction
title_fullStr	Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction
title_full_unstemmed	Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction
title_sort	analyses of nano-crystalline licovo4 prepared by solvothermal reaction
publishDate	2018
url	https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33750284297&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61730
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Analyses of nano-crystalline LiCoVO4 prepared by solvothermal reaction

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