Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent

Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent

Li1-xNi1+xO2was prepared by a polymerized complex method using succinic acid as a complexing agent. Ethanolic solutions of lithium acetate dihydrate, nickel acetate tetrahydrate, and succinic acid were mixed to form carboxylate precursors, which were subsequently calcined at 650-800°C for 14-48 h. T...

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Main Authors: Titipun Thongtem, Somchai Thongtem
Format: Journal
Published: 2018
Subjects:
Materials Science
Online Access:https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33644822976&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/61765
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Institution: Chiang Mai University
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spelling th-cmuir.6653943832-617652018-09-11T08:58:48Z Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent Titipun Thongtem Somchai Thongtem Materials Science Li1-xNi1+xO2was prepared by a polymerized complex method using succinic acid as a complexing agent. Ethanolic solutions of lithium acetate dihydrate, nickel acetate tetrahydrate, and succinic acid were mixed to form carboxylate precursors, which were subsequently calcined at 650-800°C for 14-48 h. TGA curves of metal acetates, succinic acid, and the precursors were characterized to determine weight loss and formation temperature of the oxide. By using XRD, SEM, and EDX, pure crystals of Li1-xNi1+xO2were detected at 750 and 800°C. The maximum and minimum intensity ratios of XRD spectra show that the optimum calcination condition is 750°C for 40 h. At 650-800°C, the particle size distribution is in the range of 0.35-39 μm. © Pleiades Publishing, Inc., 2006. 2018-09-11T08:58:48Z 2018-09-11T08:58:48Z 2006-01-01 Journal 16083172 00201685 2-s2.0-33644822976 10.1134/S0020168506020166 https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33644822976&origin=inward http://cmuir.cmu.ac.th/jspui/handle/6653943832/61765
institution Chiang Mai University
building Chiang Mai University Library
country Thailand
collection CMU Intellectual Repository
topic Materials Science
spellingShingle Materials Science
Titipun Thongtem
Somchai Thongtem
Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent
description Li1-xNi1+xO2was prepared by a polymerized complex method using succinic acid as a complexing agent. Ethanolic solutions of lithium acetate dihydrate, nickel acetate tetrahydrate, and succinic acid were mixed to form carboxylate precursors, which were subsequently calcined at 650-800°C for 14-48 h. TGA curves of metal acetates, succinic acid, and the precursors were characterized to determine weight loss and formation temperature of the oxide. By using XRD, SEM, and EDX, pure crystals of Li1-xNi1+xO2were detected at 750 and 800°C. The maximum and minimum intensity ratios of XRD spectra show that the optimum calcination condition is 750°C for 40 h. At 650-800°C, the particle size distribution is in the range of 0.35-39 μm. © Pleiades Publishing, Inc., 2006.
format Journal
author Titipun Thongtem
Somchai Thongtem
author_facet Titipun Thongtem
Somchai Thongtem
author_sort Titipun Thongtem
title Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent
title_short Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent
title_full Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent
title_fullStr Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent
title_full_unstemmed Characterization of Li 1-xNi 1+xO 2 prepared using succinic acid as a complexing agent
title_sort characterization of li 1-xni 1+xo 2 prepared using succinic acid as a complexing agent
publishDate 2018
url https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=33644822976&origin=inward
http://cmuir.cmu.ac.th/jspui/handle/6653943832/61765
_version_ 1681425681704026112

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