Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent
Double-sheaves of antimony sulfide were synthesized by the 200 °C and 24 h hydrothermal reaction in the acidic solution, containing copolymer - a crystal splitting agent. Using X-ray technique, electron microscopy, and Raman as well as UV-visible NIR absorption spectroscopy, the products were specif...
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th-cmuir.6653943832-61942014-08-30T03:23:56Z Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent Pilapong C. Thongtem T. Thongtem S. Double-sheaves of antimony sulfide were synthesized by the 200 °C and 24 h hydrothermal reaction in the acidic solution, containing copolymer - a crystal splitting agent. Using X-ray technique, electron microscopy, and Raman as well as UV-visible NIR absorption spectroscopy, the products were specified as orthorhombic Sb2S3, composing of Sb and S with five vibration modes, in the shape of spears in bundles with the [0 0 1] growth direction and 2.38 eV direct energy gap. A diffraction pattern was also simulated, and is in good accordance with that obtained by the interpretation. © 2010 Elsevier B.V. All rights reserved. 2014-08-30T03:23:56Z 2014-08-30T03:23:56Z 2010 Article 9258388 10.1016/j.jallcom.2010.08.003 JALCE http://www.scopus.com/inward/record.url?eid=2-s2.0-77957103934&partnerID=40&md5=aaa9676c065fe69e4ca8155d02b55018 http://cmuir.cmu.ac.th/handle/6653943832/6194 English |
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Double-sheaves of antimony sulfide were synthesized by the 200 °C and 24 h hydrothermal reaction in the acidic solution, containing copolymer - a crystal splitting agent. Using X-ray technique, electron microscopy, and Raman as well as UV-visible NIR absorption spectroscopy, the products were specified as orthorhombic Sb2S3, composing of Sb and S with five vibration modes, in the shape of spears in bundles with the [0 0 1] growth direction and 2.38 eV direct energy gap. A diffraction pattern was also simulated, and is in good accordance with that obtained by the interpretation. © 2010 Elsevier B.V. All rights reserved. |
| format |
Article |
| author |
Pilapong C. Thongtem T. Thongtem S. |
| spellingShingle |
Pilapong C. Thongtem T. Thongtem S. Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent |
| author_facet |
Pilapong C. Thongtem T. Thongtem S. |
| author_sort |
Pilapong C. |
| title |
Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent |
| title_short |
Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent |
| title_full |
Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent |
| title_fullStr |
Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent |
| title_full_unstemmed |
Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent |
| title_sort |
hydrothermal synthesis of double sheaf-like sb2s3 using copolymer as a crystal splitting agent |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-77957103934&partnerID=40&md5=aaa9676c065fe69e4ca8155d02b55018 http://cmuir.cmu.ac.th/handle/6653943832/6194 |
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