Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation
Nanocrystalline compounds MMoO4 (M = Ca, Sr and Ba) were synthesized in propylene glycol using cyclic microwave radiation. XRD, TEM, SAED and EDX analyses revealed the presence of nanocrystallites of the phases containing the corresponding alkaline earth metals, Mo and O. The calculated lattice para...
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th-cmuir.6653943832-62092014-08-30T03:23:58Z Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation Phuruangrat A. Thongtem T. Thongtem S. Nanocrystalline compounds MMoO4 (M = Ca, Sr and Ba) were synthesized in propylene glycol using cyclic microwave radiation. XRD, TEM, SAED and EDX analyses revealed the presence of nanocrystallites of the phases containing the corresponding alkaline earth metals, Mo and O. The calculated lattice parameters and the crystallite sizes both increased with the increase in the atomic masses and the ionic radii of the divalent metals. Six different vibrations were detected using Raman spectroscopy, and very strong Mo-O stretching mode of [MoO4]2- tetrahedrons was observed using FTIR. 2014-08-30T03:23:58Z 2014-08-30T03:23:58Z 2010 Article 1371339 http://www.scopus.com/inward/record.url?eid=2-s2.0-77956622992&partnerID=40&md5=217784ac93a78a37fcbdf8211f4d1134 http://cmuir.cmu.ac.th/handle/6653943832/6209 English |
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English |
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Nanocrystalline compounds MMoO4 (M = Ca, Sr and Ba) were synthesized in propylene glycol using cyclic microwave radiation. XRD, TEM, SAED and EDX analyses revealed the presence of nanocrystallites of the phases containing the corresponding alkaline earth metals, Mo and O. The calculated lattice parameters and the crystallite sizes both increased with the increase in the atomic masses and the ionic radii of the divalent metals. Six different vibrations were detected using Raman spectroscopy, and very strong Mo-O stretching mode of [MoO4]2- tetrahedrons was observed using FTIR. |
| format |
Article |
| author |
Phuruangrat A. Thongtem T. Thongtem S. |
| spellingShingle |
Phuruangrat A. Thongtem T. Thongtem S. Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation |
| author_facet |
Phuruangrat A. Thongtem T. Thongtem S. |
| author_sort |
Phuruangrat A. |
| title |
Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation |
| title_short |
Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation |
| title_full |
Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation |
| title_fullStr |
Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation |
| title_full_unstemmed |
Synthesis of nanocrystalline metal molybdates using cyclic microwave radiation |
| title_sort |
synthesis of nanocrystalline metal molybdates using cyclic microwave radiation |
| publishDate |
2014 |
| url |
http://www.scopus.com/inward/record.url?eid=2-s2.0-77956622992&partnerID=40&md5=217784ac93a78a37fcbdf8211f4d1134 http://cmuir.cmu.ac.th/handle/6653943832/6209 |
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1681420570831355904 |